A facile synthesis of 3-aryl-2-mercaptoacrylic acid under microwave irradiation

被引：3
|
作者：
Zhou, Jian-Feng [1 ,2 ]
Zhu, Feng-Xia [2 ]
Zhu, Hui-Qin [2 ]
Zhu, Yu-Lan [1 ,2 ]
机构：
[1] Huaiyin Teachers Coll, Dept Chem, Huaian 223300, Peoples R China
[2] Jiangsu Key Lab Chem Low Dimens Mat, Huaian 223300, Peoples R China
来源：
ARKIVOC | 2007年
关键词：
rhodanine; benzylidenerhodanines; 3-aryl-2-mercaptoacrylic acids; microwave irradiation;
D O I：
10.3998/ark.5550190.0008.e20
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A series of 3-aryl-2-mercaptoacrylic acid derivatives were synthesized by the hydrolysis of 5-(benzylidene) rhodanines in alkaline solution under microwave irradiation. Compared with the classical reaction conditions, this method has the advantage of excellent yields (75 similar to 94%), short reaction time (3 similar to 6 min), environmental benign, low energy consumption and easy work-up.
引用
收藏
页码：213 / 217
页数：5
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