Fast detection of raticides by Fourier transform infrared spectrometry and gas chromatography-mass spectrometry

被引：0

作者：

Cai, XL

Wu, GP

Zhang, DM

Ju, HX ^{[1
]}

机构：

[1] Nanjing Univ, Dept Chem, Inst Analyt Sci, State Key Lab Coordinat Chem, Nanjing 210093, Peoples R China

[2] Jiangsu Publ Secur Coll, Dept Technol, Nanjing 210012, Peoples R China

来源：

CHINESE JOURNAL OF ANALYTICAL CHEMISTRY | 2003年 / 31卷 / 07期

关键词：

Fourier transform infrared spectroscopy; gas chromatography/mass spectrometry; tetramint; fluoroacetamide;

D O I：

暂无

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

This paper presented the standard mass spectra of tetramint (TEM) and fluoroacetamide by subtractive spectroscopic technique of Fourier transform infrared spectrometry (FTIR) and specific ion monitoring technique of gas chromatography-mass spectrometry (GC/MS). A novel method for the fast detection of raticides was established by combining the extraction by organic solvent with FTIR and GUMS techniques. The identification of 7 samples showed a satisfactory result. This work provided a quick, simple and effective method for cracking the criminal cases related to TEM, fluoroacetamide as well as their mixture.

引用

页码：836 / 839

页数：4

共 10 条

[1] DETERMINATION OF SODIUM FLUOROACETATE (COMPOUND 1080) IN BIOLOGICAL TISSUES
ALLENDER, WJ
[J]. JOURNAL OF ANALYTICAL TOXICOLOGY, 1990, 14 (01) : 45 - 49
[2] CASPER HH, 1985, J ASSOC OFF ANA CHEM, V68, P722
[3] FENG SZ, 1999, NAT S DET METH RAT, P9
[4] Guang F Y, 1995, ENVIRON CHEM, V14, P196
[5] HU NZ, 1983, NEW DRUG ANAL CHEM, P451
[6] LIU JL, 1987, CHEM B, P1
[7] OKUMO I, 1984, J ASSOC OFF ANA CHEM, V67, P549
[8] OKUMO I, 1982, J ASSOC OFF ANA CHEM, V65, P1102
[9] WU JG, 1994, CONT TECHNOLOGY APPL, P122
[10] ZHANG L, 1994, CHIN J PHARMACOEPIDE, V3, P4

← 1 →