Preparation of silica-based aerogels by supercritical drying

被引:9
|
作者
Men'shutina, N. V. [1 ]
Katalevich, A. M. [1 ]
Smirnova, I. [2 ]
机构
[1] Mendeleev Univ Chem Technol Russia, Moscow, Russia
[2] Hamburg Univ Technol, Hamburg, Germany
关键词
supercritical drying; autoclave; sol-gel technology; aerogel; PORE VOLUME;
D O I
10.1134/S1990793114070100
中图分类号
O64 [物理化学(理论化学)、化学物理学]; O56 [分子物理学、原子物理学];
学科分类号
070203 ; 070304 ; 081704 ; 1406 ;
摘要
A technique to improve the environmental friendliness of the preparation of aerogels has been proposed; an experimental setup for supercritical drying of aerogels has been designed. The results of the examination of the aerogels prepared by the proposed technique have been described.
引用
收藏
页码:973 / 979
页数:7
相关论文
共 50 条
  • [1] Preparation of silica-based aerogels by supercritical drying
    N. V. Men’shutina
    A. M. Katalevich
    I. Smirnova
    [J]. Russian Journal of Physical Chemistry B, 2014, 8 : 973 - 979
  • [2] PREPARATION OF SILICA AEROGELS BY SUPERCRITICAL DRYING TECHNIQUE
    CHEN, LW
    GAN, LH
    YUE, TY
    LI, GM
    WANG, J
    SHEN, J
    [J]. CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE, 1995, 16 (06): : 840 - 843
  • [3] Supercritical drying with zeolite for the preparation of silica aerogels
    Yoda, S
    Ohshima, S
    Ikazaki, F
    [J]. JOURNAL OF NON-CRYSTALLINE SOLIDS, 1998, 231 (1-2) : 41 - 48
  • [4] Preparation of silica aerogels by non-supercritical drying
    Gan, LH
    Chen, LW
    Zhang, YX
    [J]. ACTA PHYSICO-CHIMICA SINICA, 2003, 19 (06) : 504 - 508
  • [5] Preparation of monolithic silica-based aerogels with high thermal stability by ambient pressure drying
    Ji, Xiaofei
    Zhou, Qian
    Qiu, Guibo
    Yue, Changsheng
    Guo, Min
    Chen, Fangqin
    Zhang, Mei
    [J]. CERAMICS INTERNATIONAL, 2018, 44 (11) : 11923 - 11931
  • [6] The application of supercritical drying in the synthesis of silica-based materials
    Puzynin, A. I.
    [J]. RUSSIAN JOURNAL OF PHYSICAL CHEMISTRY B, 2014, 8 (07) : 944 - 952
  • [7] The application of supercritical drying in the synthesis of silica-based materials
    A. I. Puzynin
    [J]. Russian Journal of Physical Chemistry B, 2014, 8 : 944 - 952
  • [8] Preparation of block silica aerogels via non-supercritical drying
    Lin, Gao-Yong
    Zhang, Dong
    Lu, Bin
    [J]. Zhongnan Daxue Xuebao (Ziran Kexue Ban)/Journal of Central South University (Science and Technology), 2006, 37 (06): : 1117 - 1121
  • [9] Preparation and Characterization of Ultralow Density Silica Aerogels by Acetonitrile Supercritical Drying
    Liu, Guangwu
    Ni, Xingyuan
    Zhou, Bin
    Yu, Qiujie
    [J]. MATERIALS FOR ENERGY CONVERSION AND STORAGE, 2012, 519 : 83 - 86
  • [10] SILICA AEROGELS PREPARED BY THE SUPERCRITICAL DRYING TECHNIQUE
    IURA, J
    [J]. JOURNAL DE PHYSIQUE, 1989, 50 (C-4): : C453 - C458