Hydrothermal Aging Behavior of Nanocrystalline Y-TZP Ceramics

被引:49
|
作者
Paul, Anish [1 ]
Vaidhyanathan, Bala [1 ]
Binner, Jon G. P. [1 ]
机构
[1] Univ Loughborough, Dept Mat, Loughborough LE11 3TU, Leics, England
基金
英国工程与自然科学研究理事会;
关键词
TETRAGONAL ZIRCONIA POLYCRYSTAL; YTTRIA-STABILIZED ZIRCONIA; FRACTURE-TOUGHNESS; GRAIN-SIZE; MECHANICAL-PROPERTIES; PHASE-TRANSFORMATION; VICKERS INDENTATION; ZRO2; POLYCRYSTALS; DEGRADATION; WATER;
D O I
10.1111/j.1551-2916.2010.04341.x
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
The influence of grain size and yttria content on the hydrothermal aging behavior of yttria-stabilized zirconia ceramics has been investigated via the preparation of genuine, fully dense nanozirconia ceramics with <100 nm grain size by two-step sintering. The samples were aged at different temperatures for varying periods of time and XRD and micro-Raman spectroscopy have been used to monitor the aging process while the hardness of the samples was used as a measure of the deterioration in the physical properties. The results were compared with those of a commercial submicrometer 3YSZ zirconia sample subjected to the same aging treatment and characterization. Nano3YSZ with <100 nm grain size did not exhibit degradation, whereas the submicrometer 3YSZ samples underwent severe degradation.
引用
收藏
页码:2146 / 2152
页数:7
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