IR and NMR spectroscopic characterization of graphitization process occurring in the pores of mesoporous silicates in formation of carbon nanotubes

被引：5

作者：

Urbán, M ^{[1
]}

Kónya, Z ^{[1
]}

Méhn, D ^{[1
]}

Kiricsi, IR ^{[1
]}

机构：

[1] Univ Szeged, Appl & Environm Chem Dept, H-6720 Szeged, Hungary

来源：

JOURNAL OF MOLECULAR STRUCTURE | 2005年 / 744卷

关键词：

carbon nanotubes; Al-MCM-41; Si-MCM-41; C-13-; Si-29-; Al-27 MAS NMR; pyridine adsorption; IR spectroscopy;

D O I：

10.1016/j.molstruc.2005.01.029

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

Synthesis of carbon nanotubes (CNTs) from the template molecules of the Si-MCM-41 and Al,Si-MCM-41 mesoporous silicates were investigated. The generation of nanotubes was carried out by graphitization, i.e. applying high temperature treatment of the MCM-41 samples in inert gas atmosphere. The as-synthesized and graphitized samples were characterized by several spectroscopic and physico-chemical methods such as IR and MAS NMR spectroscopy, XRD, TEM, and BET. (c) 2005 Elsevier B.V. All rights reserved.

引用

页码：93 / 99

页数：7

共 6 条

[1] Production of carbon nanotubes inside the pores of mesoporous silicates
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CHEMICAL PHYSICS LETTERS, 2002, 359 (1-2) : 95 - 100
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