Rietveld method in the analysis of nanocrystalline lithium-manganese spinel

被引:1
|
作者
Lisovytskiy, D [1 ]
Pielaszek, J [1 ]
Baumer, VN [1 ]
机构
[1] Polish Acad Sci, Inst Phys Chem, PL-01224 Warsaw, Poland
来源
关键词
D O I
10.1142/9789812702913_0014
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The X-ray diffraction studies using Rietveld refinement method were performed on lithium - manganese spinels produced by low and high temperature sol-gel methods and on spinels obtained from industrial supplier. The low-temperature phase transition was observed for spinel obtained by sol-gel method and treated at high temperature. Average crystallite sizes as well as phase concentrations were calculated.
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页码:77 / 81
页数:5
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