(2R, 3S, 4S, 5R)-Methyl 5-cyano-2,3:4,5-di-O-isopropylidene-2,3,4,5-tetrahydroxypentanoate

被引：0
|
作者：
Glawar, A [1 ]
Mayes, BA [1 ]
Watkin, D [1 ]
Fleet, GWJ [1 ]
机构：
[1] Univ Oxford, Chem Res Lab, Dept Organ Chem, Oxford OX1 3TA, England
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2005年 / 61卷
关键词：
D O I：
10.1107/S1600536805023834
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title nitrile, C13H19NO6, a formal oxidation product, was unexpectedly isolated during hydrogenation of an azide precursor in the presence of palladium black.
引用
收藏
页码：O2727 / O2729
页数：3
相关论文
共 50 条
  • [1] (3S,4S,5R)-3-hydroxy-4-methyl-5-vinyltetrahydropyran-2-one
    Koerner, Marleen
    Schuermann, Markus
    Preut, Hans
    Hiersemann, M.
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O3012 - U3245
  • [2] (2R,3S,4S,5R)-4-hydroxy-3-iodo-5-methyltetrahydro-2-furylmethyl benzoate
    Bew, SP
    Light, ME
    Hursthouse, MB
    Knight, DW
    Middleton, RJ
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2001, 57 : O58 - O60
  • [3] Stereoselective synthesis of (2R,3S,4S,5R)-trans-3,4-dihydroxy-5-(4-fluorophenoxymethyl)-2-(1-N-hydroxyureidyl-3-butyn-4-yl)tetrahydrofuran and (2R,3S,4S,5R)-trans-5-ethynyl-2(4-fluorophenoxymethyl)-3,4-O-isopropylidene tetrahydrofuran from mannose diacetonide
    Sharma, GVM
    Punna, S
    Hymavathi, L
    Reddy, NY
    Krishna, PR
    Chorghade, MS
    Ley, SV
    [J]. TETRAHEDRON-ASYMMETRY, 2005, 16 (06) : 1135 - 1140
  • [4] An expeditious synthesis of a (3S,4S,5R)-trihydroxyazepane
    Dhavale, DD
    Chaudhari, VD
    Tilekar, JN
    [J]. TETRAHEDRON LETTERS, 2003, 44 (39) : 7321 - 7323
  • [5] (3S,4S,5R)-4-Hydroxy-3-methyl-5-[(2S,3R)-3-methylpent-4-en-2-yl]-4,5-dihydrofuran-2(3H)-one
    Gille, Annika
    Blaeser, Dieter
    Boese, Roland
    Preut, Hans
    Hiersemann, Martin
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O154 - U2600
  • [6] IDENTIFICATION AND STEREOCHEMISTRY OF (2S, 4S, 5R) AND (2R, 4S, 5R)-2,3,4-TRIMETHYL-5-PHENYLOXAZOLIDINE, DEGRADATION PRODUCTS OF EPHEDRINE
    BECKETT, AH
    JONES, GR
    [J]. TETRAHEDRON, 1977, 33 (24) : 3313 - 3316
  • [7] Synthesis of (2R,3S,4S)-4-aryl-3-hydroxyprolinols
    Chang, Meng-Yang
    Lin, Chun-Yu
    Wu, Tsun-Cheng
    [J]. TETRAHEDRON, 2006, 62 (52) : 12334 - 12339
  • [8] Asymmetric synthesis of (3S,4R,5R)-4,5-dihydroxy-3-methyl-2,3,4,5-tetrahydropyridazine:: a formal synthesis of 1-azagulofagomine analogues
    Arroyo, Y
    Rodríguez, JF
    Santos, M
    Tejedor, MAS
    Vaca, I
    Ruano, JLG
    [J]. TETRAHEDRON-ASYMMETRY, 2004, 15 (06) : 1059 - 1063
  • [9] (2S*,3R*,4S*,5R*)-3-(S*-1-Benzyloxyethyl)-4-methyl-4-nitro-5-phenylproline methyl ester
    Linden, A
    Ayerbe, M
    Arrieta, A
    Zubia, A
    Vivanco, S
    Erquicia, E
    Aldaba, E
    Cossío, FP
    Lecea, B
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2001, 57 : O1123 - O1125
  • [10] Synthesis of 3, 4-O-isopropylidene(3S,4S)-dihydroxy-(2R,5R)bis(diphenylphosphino)hexane and its application in Rh-catalyzed highly enantioselective hydrogenation of enamides
    Li, W
    Zhang, XM
    [J]. JOURNAL OF ORGANIC CHEMISTRY, 2000, 65 (18): : 5871 - 5874
12345