One-Step Synthesis of Phosphorylated Vinylacethylene Derivatives

被引：0
|
作者：
Brel, V. K. [1 ]
机构：
[1] Russian Acad Sci, AN Nesmeyanov Inst Organoelement Cpds, Moscow 119991, Russia
来源：
RUSSIAN JOURNAL OF GENERAL CHEMISTRY | 2019年 / 89卷 / 11期
基金：
俄罗斯基础研究基金会;
关键词：
organophosphorus compounds; unsaturated compounds; vinylacetylene; SOLVENT-EXTRACTION; OXIDE; PHOSPHONATES; CYCLIZATION; ANALOGS;
D O I：
10.1134/S1070363219110082
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A one-step method for the preparation of 3-substituted 2-(diethylphosphoryl)but-1-en-3-ynes was developed based on the reaction of phosphorylated alpha-allene alcohols with methanesulfonic anhydride in the presence of triethylamine. The obtained vinylacetylene derivatives are of interest as promising precursors for the creation of organophosphorus heterocyclic compounds.
引用
收藏
页码：2212 / 2218
页数：7
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