Synthesis and crystal structure of 4-(p-methoxyphenyl)-3, 5-bis(4-pyridyl)-1,2,4-triazole

被引：16
|
作者：
Zhu, DR
Zhu, XL
Xu, L
Shao, SC
Raj, SSS
Fun, HK
You, XZ [1 ]
机构：
[1] Nanjing Univ, Inst Coordinat Chem, State Key Lab Coordinat Chem, Nanjing 210093, Peoples R China
[2] Univ Sains Malaysia, Sch Phys, Xray Crystallog Unit, Penang 11800, Malaysia
来源：
JOURNAL OF CHEMICAL CRYSTALLOGRAPHY | 2000年 / 30卷 / 06期
基金：
中国国家自然科学基金;
关键词：
triazole; crystal structure;
D O I：
10.1023/A:1009542208264
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The 4-(p-methoxyphenyl)-3,5-bis(4-pyridyl)1,2,4-triazole has been synthesized and its crystal structure has been determined by X-ray diffraction methods. It crystallizes in the monoclinic space group P2(1)/n, with a = 12.5832(6) Angstrom, b = 7.0512(5) Angstrom, c = 18.4669(12) Angstrom, beta = 96.826(1)degrees, and D-calc = 1.345 g cm(-1) for Z = 4. In the structure, two pyridyl rings, phenyl ring, and triazole ring do not share a common plane. The most favored orientation of the pyridyl rings in the crystal is that their planes are inclined toward opposite directions with respect to the triazole ring.
引用
收藏
页码：429 / 432
页数：4
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