The cocrystal of 4-oxopimelic acid and 4,4′-bipyridine: polymorphism and solid-state transformations

被引：17
|
作者：
Halasz, Ivan [1 ]
Rubcic, Mirta [1 ]
Uzarevic, Krunoslav [1 ]
Dilovic, Ivica [1 ]
Mestrovic, Ernest [1 ]
机构：
[1] Univ Zagreb, Fac Sci, Dept Chem, Zagreb 10000, Croatia
来源：
NEW JOURNAL OF CHEMISTRY | 2011年 / 35卷 / 01期
关键词：
CO-CRYSTAL; PHARMACEUTICAL COCRYSTALS; CARBOXYLIC-ACIDS; HYDROGEN-BOND; CONFORMATIONAL POLYMORPHISM; STRUCTURAL-CHARACTERIZATION; PHYSICOCHEMICAL PROPERTIES; SUPRAMOLECULAR SYNTHONS; ORGANIC-SYNTHESIS; MECHANISM;
D O I：
10.1039/c0nj00569j
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The cocrystal of 4-oxopimelic acid and 4,4'-bipyridine was isolated in two polymorphic forms depending upon the solvent of crystallisation. Polymorphs exhibit hydrogen-bonded chains formed between the carboxyl and pyridine moieties while different packing arrangements of chains result from C-H center dot center dot center dot O interactions. Solid-state synthesis and interconversion conditions were investigated by grinding and thermal methods.
引用
收藏
页码：24 / 27
页数：4
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