Synthesis and characterization of nanocrystalline SnO2 powder

被引：1
|
作者：
Liu, Shi-min [1 ]
Ding, Wan-yu [2 ]
Jiang, Wei-wei [3 ]
Chai, Wei-ping
机构：
[1] Dalian Jiaotong Univ, Sch Mat Sci & Engn, Dalian 116028, Peoples R China
[2] Dalian Jiaotong Univ, Inst Optoelect Mat & Devices, Dalian 116028, Peoples R China
[3] Engn Res Ctr Optoelect Mat & Devices, Dalian, 116028, Peoples R China
来源：
ADVANCED MATERIAL SCIENCE AND TECHNOLOGY, PTS 1 AND 2 | 2011年 / 675-677卷
关键词：
nanocrystalline SnO2 powder; crystallization; gas sensitivity; TIN OXIDE NANOPARTICLES; GAS-SENSING PROPERTIES;
D O I：
10.4028/www.scientific.net/MSF.675-677.267
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
Nanocrystalline SnO2 powder has been synthesized via direct precipitation method starting from Sn, HNO3, HCl, and NH4OH. Thermal properties, crystal structural and morphological properties of the precursor and SnO2 powder were investigated using simultaneous thermogravimetry-differential thermal analysis, X-ray diffraction and transmission electron microscopy. The results indicated that the precursor was SnO2 rather than Sn(OH)(2) or Sn(OH)(4). On the basis of the precursor, well crystallized SnO2 powder with 4-5 nm in diameter was obtained, after calcined at 350 degrees C for 2 h.
引用
收藏
页码：267 / +
页数：3
相关论文
共 50 条
  • [1] Synthesis of nanocrystalline SnO2 powder at 100°C
    Sanjay R. Dhage
    S. P. Gaikwad
    Violet Samuel
    V. Ravi
    [J]. Bulletin of Materials Science, 2004, 27 : 221 - 222
  • [2] Synthesis of nanocrystalline SnO2 powder at 100°C
    Dhage, SR
    Gaikwad, SP
    Samuel, V
    Ravi, V
    [J]. BULLETIN OF MATERIALS SCIENCE, 2004, 27 (03) : 221 - 222
  • [3] Synthesis of nanocrystalline SnO2 powder by amorphous citrate route
    Bhagwat, M
    Shah, P
    Ramaswamy, V
    [J]. MATERIALS LETTERS, 2003, 57 (9-10) : 1604 - 1611
  • [4] Synthesis and characterization of SnO2 nanobelts by carbothermal reduction of SnO2 powder
    Ni, Zi-Feng
    Ying, Peng-Zhan
    Luo, Yong
    Dai, Xin-Lian
    Liu, Tao
    [J]. JOURNAL OF INORGANIC MATERIALS, 2007, 22 (04) : 609 - 612
  • [5] Synthesis and Characterization of Ni Doped SnO2 Powder
    Yang Fanger
    Qiu Kaifeng
    Zhang Ji
    Cai Jiangnan
    Zheng Xiaohua
    Zhang Lingjie
    Shen Tao
    [J]. RARE METAL MATERIALS AND ENGINEERING, 2016, 45 : 564 - 566
  • [6] Synthesis of nanocrystalline SnO2 by precipitation
    Dong, X.
    Tian, H.
    Zhang, W.
    Liu, G.
    Hong, Y.
    Hong, G.
    [J]. Binggong Xuebao/Acta Armamentarii, 2001, 22 (02): : 244 - 247
  • [7] Synthesis of nanocrystalline SnO2 in supercritical water
    Zhen Fang
    Hassane Assaaoudi
    Hanbai Lin
    Xiaoming Wang
    Ian S. Butler
    Janusz A. Kozinski
    [J]. Journal of Nanoparticle Research, 2007, 9 : 683 - 687
  • [8] Synthesis of nanocrystalline SnO2 in supercritical water
    Fang, Zhen
    Assaaoudi, Hassane
    Lin, Hanbai
    Wang, Xiaoming
    Butler, Ian S.
    Kozinski, Janusz A.
    [J]. JOURNAL OF NANOPARTICLE RESEARCH, 2007, 9 (04) : 683 - 687
  • [9] Morphologically selective synthesis of nanocrystalline SnO2
    Liu, Y
    Yang, GC
    Zhang, XT
    Bai, YB
    Li, TJ
    [J]. CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE, 2000, 21 (10): : 1569 - 1571
  • [10] Synthesis of nanocrystalline SnO2 powder from SnCl4 by mechanochemical processing
    Billik, P.
    Caplovicova, M.
    [J]. POWDER TECHNOLOGY, 2009, 191 (03) : 235 - 239
12345