1,5-[5,5′-(3-oxa-1,5-pentylenedithio)bis(2,3-dihydro-2-oxo-1,3,4-thiadiazol-3-yl)]-3-oxapentane

被引：4
|
作者：
Cho, NS
Hong, SI
Kim, JG
Suh, IH [1 ]
机构：
[1] Chungnam Natl Univ, Dept Phys, Taejon 305764, South Korea
[2] Chungnam Natl Univ, Dept Chem, Taejon 305764, South Korea
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2001年 / 57卷
关键词：
D O I：
10.1107/S1600536801006250
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title compound, 4,14-dioxa-9,11,17,19-tetrathia-1,7,21,22-tetraazatricyclo[16.2.1.1(7,10)]docosa-18(21),10(22)-diene-8,20-dione, C12H16N4O4S4, has crystallographic twofold symmetry, with a half molecule in the asymmetric unit and a dihedral angle of 52.59 (6)degrees between the two planar five-membered rings of the macrocycle, giving the molecule a twisted conformation.
引用
收藏
页码：O434 / O435
页数：2
相关论文
共 50 条
  • [1] 1,5-[5,5′-(1,3-phenylenedimethylenedithio)bis(2,3-dihydro-2-oxo-1,3,4-thiadiazol-3-yl)]-3-oxapentane
    Cho, NS
    Hong, SI
    Choo, GH
    Kim, JG
    Suh, IH
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2001, 57 : o368 - o369
  • [2] Synthesis and structure of 1,3-[5,5′-(1,2-phenylenedimethylenedithio)bis-(2,3-dihydro-2-oxo-1,3,4-thiadiazol-3-yl]propane
    Cho, NS
    Park, CK
    Hwang, HJ
    Hong, SI
    Kim, JG
    Suh, IH
    [J]. JOURNAL OF CHEMICAL RESEARCH-S, 1999, (12): : 730 - 731
  • [3] 1,5-bis(2-formylphenoxy)-3-oxapentane
    Dionysio, Nivea C. F.
    Bordinhao, Jairo
    Visentin, Lorenzo do Canto
    Ronconi, Celia Machado
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O546 - U717
  • [4] Methidathion: S-(5-methoxy-2-oxo-2,3-dihydro-1,3,4-thiadiazol-3-yl)methyl O,O-dimethyl phosphorodithioate
    Kim, Hyunjee
    Shin, Yong Woon
    Park, Ki-Min
    Kim, Jineun
    Kim, Tae Ho
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O653 - U2037
  • [5] 1-(5-Benzylsulfanyl-2,2-dimethyl-2,3-dihydro-1,3,4-thiadiazol-3-yl)-2,2-dimethylpropan-1-one
    Yusof, Mohd Sukeri Mohd
    Mutalib, Fatimah Abdul
    Arshad, Suhana
    Razak, Ibrahim Abdul
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1228 - +
  • [6] 5-({3-[(5-Amino-1,3,4-thiadiazol-2-yl)-sulfanylmethyl]benzyl}sulfanyl)-1,3,4-thiadiazol-2-amine
    Kang, Sung Kwon
    Cho, Nam Sook
    Jang, Siyoung
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : 1241 - +
  • [7] N-(3-Cyano-4,5,6,7-tetrahydrobenzothiophen-2-yl)-2-[[5-[(1,5-dimethyl-3-oxo-2-phenylpyrazol-4-yl)amino]-1,3,4-thiadiazol-2-yl]sulfanyl]acetamide
    Holota, Serhii
    Yushyn, Ihor
    Khyluk, Dmytro
    Vynnytska, Renata
    Lesyk, Roman
    [J]. MOLBANK, 2021, 2021 (02)
  • [8] 5,5′-[methylenebis(sulfanediyl)]bis(1,3,4-thiadiazol-2-amine)
    Meng, Fankun
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O2000 - U4451
  • [9] 2-[5-(Cyclohexylamino)-1,3,4-thiadiazol-2-yl]phenol
    Seena, E. B.
    Kurup, M. R. Prathapachandra
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O5627 - O5629
  • [10] 1,5-Di(tetrazol-5-yl)-3-oxapentane as a substrate in the synthesis of novel heterocyclic systems
    Zubarev, VY
    Filichev, VV
    Trifonov, RE
    Ostrovskii, VA
    [J]. MENDELEEV COMMUNICATIONS, 1999, (03) : 116 - 117
12345