Low temperature hydrothermal synthesis of nano-sized manganese oxide for supercapacitors

被引:56
|
作者
Liu, Jing-Liang [1 ]
Fan, Li-Zhen [1 ]
Qu, Xuanhui [1 ]
机构
[1] Univ Sci & Technol Beijing, Sch Mat Sci & Engn, Beijing 100083, Peoples R China
基金
中国国家自然科学基金;
关键词
Manganese oxide; Supercapacitors; Hydrothermal synthesis; Nano-structure; Specific capacitance; ELECTROCHEMICAL PROPERTIES; MNO2; GROWTH; RUO2;
D O I
10.1016/j.electacta.2012.01.095
中图分类号
O646 [电化学、电解、磁化学];
学科分类号
081704 ;
摘要
The nano-structured manganese oxide was synthesized by a simple hydrothermal route at a very low temperature of 60 degrees C using potassium permanganate as oxidant and ethanol as reductant. The structure and surface morphology of the as-prepared manganese oxide were characterized by means of X-ray diffraction and scanning electron microscopy. The obtained manganese oxide was of amorphous and spherical with a particle size of about 100 nm. The capacitive characteristics of the nano-structured manganese oxide electrodes were investigated by means of cyclic voltammetry and galvanostatic charge-discharge cycling in 1 M Na2SO4. The manganese oxide exhibited not only a maximum specific capacitance of 198 Fg(-1), but also excellent rate capability and good cycle stability. (C) 2012 Elsevier Ltd. All rights reserved.
引用
收藏
页码:302 / 305
页数:4
相关论文
共 50 条
  • [1] Low Temperature Synthesis of Nano-Sized Lithium Manganese Oxide Powder by the Sol-Gel Process Using PVA
    Chung-Hsin Lu
    Susanta Kumar Saha
    Journal of Sol-Gel Science and Technology, 2001, 20 : 27 - 34
  • [2] Low temperature synthesis of nano-sized lithium manganese oxide powder by the sol-gel process using PVA
    Lu, CH
    Saha, SK
    JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY, 2001, 20 (01) : 27 - 34
  • [3] Low-temperature hydrothermal synthesis and structure control of nano-sized CePO4
    Bao, Jinrong
    Yu, Ranbo
    Zhang, Jiayun
    Yang, Xiaodan
    Wang, Dan
    Deng, Jinxia
    Chen, Jun
    Xing, Xianran
    CRYSTENGCOMM, 2009, 11 (08): : 1630 - 1634
  • [4] Low temperature synthesis of zircon from silicone resins and oxide nano-sized particles
    Parcianello, G.
    Bernardo, E.
    Colombo, P.
    JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2012, 32 (11) : 2819 - 2824
  • [5] Hydrothermal synthesis of nano-sized iron oxide crystals in the cavity of carbon nanotubes
    Matsui, K
    Kyotani, T
    Tomita, A
    MOLECULAR CRYSTALS AND LIQUID CRYSTALS, 2002, 387 : 225 - 229
  • [6] Hydrothermal synthesis of nano-sized iron oxide crystals in the cavity of carbon nanotubes
    Matsui, Keitaro
    Kyotani, Takashi
    Tomita, Akira
    2002, Taylor and Francis Ltd. (387) : 1 - 5
  • [7] Hydrothermal synthesis of nano-sized MnO2 supported on attapulgite electrode materials for supercapacitors
    Lin, Tao
    Lin, Jiacheng
    Wei, Xiaoyao
    Lu, Lulu
    Yin, Xuefeng
    INTERNATIONAL JOURNAL OF HYDROGEN ENERGY, 2023, 48 (29) : 10765 - 10777
  • [8] Synthesis and Vibration Spectroscopy of Nano-Sized Manganese Oxides
    Mironova-Ulmane, N.
    Kuzmin, A.
    Skvortsova, V.
    Chikvaidze, G.
    Sildos, I.
    Grabis, J.
    Jankovica, D.
    Dindune, A.
    Maiorov, M.
    ACTA PHYSICA POLONICA A, 2018, 133 (04) : 1013 - 1016
  • [9] Low-temperature synthesis of nano-sized metal molybdate powders
    Sen, A
    Pramanik, P
    MATERIALS LETTERS, 2001, 50 (5-6) : 287 - 294
  • [10] Pathways for the low temperature synthesis of nano-sized crystalline barium zirconate
    Phule, Pradeep P.
    Grundy, David C.
    Materials science & engineering. B, Solid-state materials for advanced technology, 1994, B23 (01): : 29 - 35