Microwave assisted sintering of CaCu3Ti4O12

被引:32
|
作者
Hutagalung, Sabar D. [1 ]
Ikhwan, M. [1 ]
Ibrahim, M. [1 ]
Ahmad, Zainal A. [1 ]
机构
[1] Univ Sains Malaysia, Sch Mat & Mineral Resources Engn, Nibong Tebal 14300, Penang, Malaysia
关键词
microwave processing; grain boundaries; dielectric properties; perovskites;
D O I
10.1016/j.ceramint.2007.09.074
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
CaCu3Ti4O12 electroceramic was prepared by a microwave assisted solid-state reaction technique from CaCO3, CuO and TiO2 powders. Processing involved the preparation of raw material, mixing and milling, calcination, pellet forming and sintering processes. Conventional furnace and microwave assisted sintering processes were employed in order to improve phase structures, morphology and dielectric properties of CaCu3Ti4O12 ceramics. Surface and fracture FESEM analysis showed that the microwave assisted sintered CaCu3Ti4O12 produced better densification and more uniform grain size compared to the conventional sintered sample. (c) 2007 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
引用
收藏
页码:939 / 942
页数:4
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