Synthesis and characterization of 2-deoxy-2-nicotinoylamido-ß-D-glucopyranose

被引：0
|
作者：
Guo, ZC [1 ]
Dong, YM
Xiong, XQ
Zhao, YQ
机构：
[1] Hunan Univ Sci & Technol, Fac Chem & Chem Engn, Xiangtan 411201, Hunan, Peoples R China
[2] Xiamen Univ, Dept Mat Sci & Engn, State Key Lab Phys Chem Solid Surfaces, Xiamen 361005, Fujian, Peoples R China
[3] Chinese Acad Sci, Inst Chem, Beijing 100080, Peoples R China
来源：
CHINESE JOURNAL OF CHEMISTRY | 2005年 / 23卷 / 02期
关键词：
nicotinic acid; nicotinic amide; ss-D-glucosamine hydrochloride;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A new nicotinic acid derivative, 2-deoxy-2-nicotinoylamido-beta-D-glucopyranose, was synthesized with beta-configuration exclusively. The structure and properties of the product were characterized by H-1 NMR, FT-IR, MS, DSC and polarimeter. The details of H-1 NMR spectrum and the mass spectrum proved that there are a great amount of hydrogen bonds in the product.
引用
收藏
页码：190 / 193
页数：4
相关论文
共 50 条
  • [1] 1,6-anhydro-2-iodo-2-deoxy-β-D-glucopyranose (lodolevoglucosan)
    Gehle, D
    Flörke, U
    Krohn, K
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O664 - O666
  • [2] A facile synthesis of Cerny epoxides and selectively blocked derivatives of 2-azido-2-deoxy-β-D-glucopyranose
    Xue, J
    Guo, ZW
    [J]. TETRAHEDRON LETTERS, 2001, 42 (37) : 6487 - 6489
  • [3] Co-crystals of 3-deoxy-3-fluoro-α-d-glucopyranose and 3-deoxy-3-fluoro-β-d-glucopyranose
    Zhang, Wenhui
    Oliver, Allen G.
    Serianni, Anthony S.
    [J]. ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 2010, 66 : O557 - O560
  • [4] 4-Deoxy-4-fluoro-β-d-glucopyranose
    Zhang, Wenhui
    Oliver, Allen G.
    Serianni, Anthony S.
    [J]. ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 2010, 66 : o496 - o498
  • [5] SYNTHESIS OF 1-0-(2',4'-DICHLOROPHENOXYACETYL)-D-GLUCOPYRANOSE
    KOBAYASHI, A
    WATANABE, K
    YAMASHITA, K
    [J]. AGRICULTURAL AND BIOLOGICAL CHEMISTRY, 1972, 36 (12): : 2151 - 2156
  • [6] Improved synthesis and characterization of 1,3,4,6-tetra-O-acetyl-2-(N-acetylacetamido)-2deoxy-β-D-glucopyranose
    Suihko, M
    Ahlgrén, M
    Aulaskari, P
    Rouvinen, J
    [J]. CARBOHYDRATE RESEARCH, 2001, 334 (04) : 337 - 341
  • [7] D-GLUCOPYRANOSE 6-DEOXY-6-PHOSPHONIC ACID
    SMITHGRIFFIN, B
    BURGER, A
    [J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1956, 78 (10) : 2336 - 2338
  • [8] 3-Deoxy-β-D-ribo-hexopyranose (3-deoxy-β-D-glucopyranose)
    Zhang, Wenhui
    Noll, Bruce C.
    Serianni, Anthony S.
    [J]. ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 2007, 63 : O578 - O581
  • [9] ACETOLYSIS OF O-TETRAACETYL-1-DEOXY-1-(2',4'-DI-NITROPHENYLHYDRAZINO)-D-GLUCOPYRANOSE
    GERECS, A
    [J]. ACTA CHIMICA ACADEMIAE SCIENTARIUM HUNGARICAE, 1975, 84 (04): : 467 - 469
  • [10] Synthesis of poly(2,3,4-tri-O-acetyl-α/β-D-glucopyranose)
    Fu, Liye
    Xu, Yi
    Li, Lingyao
    Du, Wenjun
    [J]. ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2013, 245
12345