Sample preparation techniques based on combustion reactions in closed vessels - A brief overview and recent applications

被引：126
|
作者：
Flores, Erico M. M. [1 ]
Barin, Juliano S.
Mesko, Marcia F.
Knapp, Guenter
机构：
[1] Univ Fed Santa Maria, Dept Quim, BR-97105 Santa Maria, RS, Brazil
[2] Graz Univ Technol, Micro & Radiochem, A-8010 Graz, Austria
来源：
SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY | 2007年 / 62卷 / 09期
关键词：
sample preparation; combustion techniques; combustion bomb; oxygen flask; microwave-induced combustion;
D O I：
10.1016/j.sab.2007.04.018
中图分类号：
O433 [光谱学];
学科分类号：
0703 ; 070302 ;
摘要：
In this review, a general discussion of sample preparation techniques based on combustion reactions in closed vessels is presented. Applications for several kinds of samples are described, taking into account the literature data reported in the last 25 years. The operational conditions as well as the main characteristics and drawbacks are discussed for bomb combustion, oxygen flask and microwave-induced combustion (MIC) techniques. Recent applications of MIC techniques are discussed with special concern for samples not well digested by conventional microwave-assisted wet digestion as, for example, coal and also for subsequent determination of halogens. (C) 2007 Elsevier B.V. All rights reserved.
引用
收藏
页码：1051 / 1064
页数：14
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