GREEN SYNTHESIS AND CHARACTERIZATION OF SILVER/SILVER OXIDE NANOPARTICLES USING AQUEOUS LEAVES EXTRACT OF ARTEMISIA HERBA-ALBA AS REDUCING AND CAPPING AGENTS

被引:0
|
作者
Belaiche, Yassine [1 ,3 ]
Khelef, Abdelhamid [2 ,3 ]
Laouini, Salah Eddine [1 ,3 ]
Bouafia, Abderrhmane [1 ,3 ]
Tedjani, Mohammed Laid [1 ,3 ]
Barhoum, Ahmed [4 ,5 ]
机构
[1] Univ Echahid Hamma Lakhdar El Oued, Fac Technol, Dept Proc Engn & Petrochem, Ei Oued 39000, Algeria
[2] Univ Echahid Hamma Lakhdar El Oued, Fac Exact Sci, Dept Chem, El Oued 39000, Algeria
[3] Univ El Oued, Fac Technol, Lab VTRS, El Oued 39000, Algeria
[4] Helwan Univ, Fac Sci, Chem Dept, NanoStruc Res Grp, Cairo 11795, Egypt
[5] Dublin City Univ, Fraunhofer Project Ctr, Sch Chem Sci, Dublin D09 V209, Ireland
关键词
silver/silver oxide nanoparticles; Artemisia Herba-Alba; Silver nitrate AgNO3; Green Synthesis; XRD; SILVER NANOPARTICLES; BIOLOGICAL SYNTHESIS; BIOSYNTHESIS; NANOCOMPOSITE;
D O I
暂无
中图分类号
TU [建筑科学];
学科分类号
0813 ;
摘要
Artemisia herba-alba is a medicinal plant, and its essential oil is used as an antiseptic and antispasmodic. In this study, green synthesis of silver/silver oxide (Ag/Ag2O) nanoparticles was successfully synthesized from Artemisia Herba-Alba aqueous leaves extract. The effect of temperature, reaction time, the concentration of AgNO3, the quantity of plant extract, and pH on the synthesis process of Ag/Ag2O was optimized. More interesting, the results showed that only 5 min were required for reducing 1 mM AgNO3 into Ag/Ag2O NPs at room temperature. The crystalline nature of Ag/Ag2O NPs with an average crystallize size of 10.736.8 nm. The green synthesizing Ag/Ag2O NPs having in general a spherical morphology with particle/aggregate size less than 100 nm. The maximum UV-Vis absorption peak of Ag/Ag2O NPs was observed at the range of 418-435 nm giving optical band gaps of 2.05-2.30 eV. The TGA/DTA analysis shows significant organic contents (18 wt%) were physically and chemically adsorbed on the dry weight Ag/Ag2O NPs. Artemisia herba-alba is a source of phytochemicals for effective and prompt fabrication of Ag/Ag2O NPs with relevant insecticidal and anti-bactericidal activity against species of high public health importance.
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页码:342 / 352
页数:11
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