Thermo-physical properties of epoxy nanocomposites reinforced with amino-functionalized multi-walled carbon nanotubes

被引:189
|
作者
Shen, Jianfeng [1 ]
Huang, Weishl [1 ]
Wu, Liping [1 ]
Hu, Yizhe [1 ]
Ye, Mingxin [1 ]
机构
[1] Fudan Univ, Dept Mat Sci, Minist Educ, Key Lab Mol Engn Polymers, Shanghai 200433, Peoples R China
关键词
thermal and mechanical properties; epoxy; amino-functionalized MWNTs;
D O I
10.1016/j.compositesa.2006.10.012
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The modification of multi-walled carbon nanotubes (MWNTs) with amine groups was investigated by FTIR, Raman spectroscopy and XPS after such steps as carboxylation, acylation and amidation. Nanotube-reinforced epoxy polymer composites were prepared by mixing amino-functionalized MWNTs with epoxy resin and curing agent. DSC, TGA, SEM and flexural test were used to investigate the thermal and mechanical properties of the composites. The results showed that amino-functionalized MWNTs could enhance tile interfacial adhesion between the nanotubes and the matrix, thus greatly improve the thermal and mechanical properties of the resin epoxy bulk material. (c) 2006 Elsevier Ltd. All rights reserved.
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页码:1331 / 1336
页数:6
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