IR spectroscopy as a quantitative and predictive analysis method of phenol-formaldehyde resol resins

被引：0
|
作者：
Holopainen, T
Alvila, L
Rainio, J
Pakkanen, TT
机构：
[1] Univ Joensuu, Dept Chem, FIN-80101 Joensuu, Finland
[2] Dynoresin Oy, FIN-82430 Puhos, Finland
来源：
JOURNAL OF APPLIED POLYMER SCIENCE | 1998年 / 69卷 / 11期
关键词：
IR spectroscopy; phenol-formaldehyde resin; resol resin; multicomponent spectroscopic;
D O I：
10.1002/(SICI)1097-4628(19980912)69:11<2175::AID-APP9>3.0.CO;2-D
中图分类号：
O63 [高分子化学（高聚物）];
学科分类号：
070305 ; 080501 ; 081704 ;
摘要：
A set of resin samples was characterized by IR and C-18-NMR spectroscopy. The suitability of IR spectroscopy for the quantitative analysis of resins was evaluated by statistical methods using the NMR reference data as calibration. The values of interesting properties, for example, the amount of free phenol and the formaldehyde-to-phenol (F/P) molar ratio, of the resins being similar to the calibration resins were predicted from the IR spectra. Also, the predicted results were compared with the ones observed by C-13-NMR spectroscopy. (C) 1998 John Wiley & Sons, Inc.
引用
收藏
页码：2175 / 2185
页数：11
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