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Porous alumina ceramics with highly aligned pores by heat-treating extruded alumina/camphene body at temperature near its solidification point
被引:25
|作者:
Moon, Young-Wook
[1
]
Shin, Kwan-Ha
[1
]
Koh, Young-Hag
[1
]
Choi, Won-Young
[2
]
Kim, Hyoun-Ee
[2
]
机构:
[1] Korea Univ, Dept Dent Lab Sci & Engn, Seoul 136703, South Korea
[2] Seoul Natl Univ, Dept Mat Sci & Engn, Seoul 151742, South Korea
关键词:
Extrusion;
Mechanical properties;
Al2O3;
Biomedical applications;
Porous ceramics;
HYDROXYAPATITE SCAFFOLDS;
MICROSTRUCTURE;
TEMPLATE;
CHANNELS;
ALCOHOL;
FORMER;
D O I:
10.1016/j.jeurceramsoc.2011.11.035
中图分类号:
TQ174 [陶瓷工业];
TB3 [工程材料学];
学科分类号:
0805 ;
080502 ;
摘要:
This study reports a novel way of increasing the pore size of highly aligned porous alumina ceramics by heat-treating an extruded alumina/camphene body at a temperature near its solidification point. The pore size obtained increased remarkably from 51 +/- 8 to 125 +/- 27 mu m with increasing heat-treatment time from 1 to 24 h, due to the continuative overgrowth of the camphene dendrites during heat-treatment, while a highly aligned porous structure was preserved. In addition, interestingly, this heat-treatment enabled alumina walls to be densified quite well, whereas porous walls were observed in the sample produced without heat-treatment, which led to a considerable increase in compressive strength. The sample produced with a heat-treatment time of 12 h showed a high compressive strength of 11.6 +/- 1.2 MPa at a porosity of approximately 84 vol%, which was much higher than that (0.28 +/- 0.1 MPa) of the sample produced without heat-treatment. (C) 2011 Elsevier Ltd. All rights reserved.
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页码:1029 / 1034
页数:6
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