Lead hexaferrite nanostructures: green amino acid sol-gel auto-combustion synthesis, characterization and considering magnetic property

被引:60
|
作者
Mahdiani, Maryam [1 ]
Sobhani, Azam [2 ]
Ansari, Fatemeh [3 ]
Salavati-Niasari, Masoud [1 ]
机构
[1] Univ Kashan, Inst Nano Sci & Nano Technol, POB 87317-51167, Kashan, Iran
[2] Kosar Univ Bojnord, Dept Chem, Bojnord, Iran
[3] Islamic Azad Univ, Sci & Res Branch, Young Res & Elites Club, Tehran, Iran
基金
美国国家科学基金会;
关键词
IRON-OXIDE NANOPARTICLES; HEXAGONAL FERRITES; PBFE12O19; NANOCOMPOSITES; POWDERS;
D O I
10.1007/s10854-017-7701-0
中图分类号
TM [电工技术]; TN [电子技术、通信技术];
学科分类号
0808 ; 0809 ;
摘要
Herein, a simple method for the synthesis of PbFe12O19 nanostructures with amino acid is reported. The nanostructures are obtained by the sol-gel auto-combustion route. The effects of type of amino acid, calcination temperature and ratio of Pb:amino acid have been optimized to achieve the best products on morphology and purity. It is the first time that valine, beta-alanine, leucine, glycine and l-cysteine are used in the synthesis of lead hexaferrites. The pure hexagonal PbFe12O19 nanostructures are formed in the presence of valine, when the molar ratio of Pb:valine is 1:13, at 900 A degrees C for 2 h. The magnetic property of the products is investigated. The lead hexaferrites with high coercive force of 5123 Oe are obtained in the presence of valine.
引用
收藏
页码:17627 / 17634
页数:8
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