Microwave-Assisted One-Pot Synthesis of 2-Amino-2-chromenes Using Piperazine as a Catalyst Under Solvent-Free Conditions

被引：32
|
作者：
Mobinikhaledi, Akbar [1 ]
Moghanian, Hassan [1 ]
Sasani, Fatemeh [1 ]
机构：
[1] Arak Univ, Fac Sci, Dept Chem, Arak 3815688349, Iran
来源：
SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY | 2011年 / 41卷 / 03期
关键词：
2-amino-2-chromenes; microwave irradiation; multicomponent; piperazine; solvent-free; AQUA MEDIATED SYNTHESIS; SUBSTITUTED; 2-AMINO-4H-CHROMENES; MULTICOMPONENT REACTIONS; HETEROCYCLIC SYNTHESIS; EFFICIENT CATALYST; COPPER NITRATE; AQUEOUS-MEDIA; DERIVATIVES; NITRILES; GREEN;
D O I：
10.1080/15533174.2011.555857
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
A simple and efficient procedure for the synthesis of substituted 2-amino-2-chromenes employing one-pot three-component condensation reaction of aromatic aldehydes with malononitrile and activated phenols has been developed by using the odorless and easy to work piperazine in the absence of solvents under microwave irradiation. The present method is operationally simple and offers several advantages such as high yields, short reaction time, and simple workup.
引用
收藏
页码：262 / 265
页数：4
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