Effect of Li2CO3 flux on the preparation temperature, particle micro morphology and light absorption performance of samarium borate by solid state method

被引：9
|
作者：
Han, Pengde [1 ]
Jiang, Xiaoping [2 ]
Zhang, Lintao [1 ]
Yu, Fangli [1 ]
Shi, Qingle [1 ]
Ding, Yujie [3 ]
Zhang, Qitu [3 ]
机构：
[1] Yancheng Inst Technol, Sch Mat Engn, Yancheng 224051, Peoples R China
[2] Yancheng Inst Technol, Analyt & Testing Ctr, Yancheng 224051, Peoples R China
[3] Nanjing Tech Univ, Coll Mat Sci & Engn, Nanjing 210009, Jiangsu, Peoples R China
来源：
JOURNAL OF MATERIALS SCIENCE-MATERIALS IN ELECTRONICS | 2015年 / 26卷 / 02期
关键词：
HYDROTHERMAL SYNTHESIS; FERRITE NANOFIBER; PHOTOLUMINESCENCE; EU3+; NANOCRYSTALS; PHOSPHOR; SMBO3; IONS;
D O I：
10.1007/s10854-014-2447-4
中图分类号：
TM [电工技术]; TN [电子技术、通信技术];
学科分类号：
0808 ; 0809 ;
摘要：
This paper modified the preparation of SmBO3 by the conventional solid state method, by using Li2CO3 as flux, to reduce the preparation temperature and improve particle quality. Characterization methods mainly used the X-ray diffraction analysis, scanning electron microscopy, light reflectivity and thermogravimetry-differential scanning calorimetry analysis. The results showed that: the usage of Li2CO3 flux effectively reduced the calcination temperature of the solid state reaction to 600 degrees C, and it improved the particle properties of SmBO3, making particle size more uniform and weakening agglomeration. The materials could absorb 1.06 and 1.54 mu m near infrared light simultaneously so it could be used as a composite absorbent. Furthermore, the mechanism of Li2CO3 flux was discussed.
引用
收藏
页码：666 / 670
页数：5
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    Pengde Han
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