Synthesis, X-ray structure and 199Hg, 77Se CP MAS NMR studies on the first tris(imidazolidine-2-selone) mercury complex:: {Chloro-tris[N-methyl-2(3H)-imidazolidine-2-selone] mercury(II)} chloride

被引：15

作者：

Al-Amri, AHD ^{[1
]}

Fettouhi, M ^{[1
]}

Wazeer, MIM ^{[1
]}

Isab, AA ^{[1
]}

机构：

[1] King Fahd Univ Petr & Minerals, Dept Chem, Dhahran 31261, Saudi Arabia

来源：

INORGANIC CHEMISTRY COMMUNICATIONS | 2005年 / 8卷 / 12期

关键词：

crystal structure; CP MAS Hg-199 NMR; Se-77; NMR; N-methyl-imidazolidine-2-selone; Hg(II) complex;

D O I：

10.1016/j.inoche.2005.09.010

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A novel cationic Hg(II) complex has been synthesized with N-methyl-imidazolidine-2-selone ligand. The tris(N-Methyl-imidazolidine2-selone) mercury(II) complex, [(MeIMSe)(3)HgCl]Cl-+(-) (1), has been characterized by single crystal X-ray analysis and CP MAS Hg-199 and Se-77 NMR. (c) 2005 Elsevier B.V. All rights reserved.

引用

页码：1109 / 1112

页数：4

共 6 条

[1] A novel polymeric Hg[(CN)2N2] central core four-coordinate complex: Synthesis, X-ray structure and 199Hg, 13C and 15N CP MAS NMR characterization of catena((μ2-1,4-diaminobutane-N,N′)dicyanomercury(II))
Al-Maythalony, Bassem A.
Fettouhi, Mohammed
Wazeer, Mohammed I. M.
Isab, Anvarhusein A.
INORGANIC CHEMISTRY COMMUNICATIONS, 2009, 12 (06) : 540 - 543
[2] Structural characteristics of three-coordinate arylhalide tellurium(II) complexes with chalcogen ligands. Synthesis, spectroscopic characterization and X-ray structural studies of bromo[N-methylbenzothiazole-2(3H)-selone]phenyltellurium(II), bromophenyl[tris(dimethylamino)phosphaneselenide]-tellurium(II) and tris(dimethylamino)phosphanesulfide
Rudd, MD
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ACTA CHEMICA SCANDINAVICA, 1996, 50 (09): : 759 - 774
[3] Structural Characteristics of Three- Coordinate Arylhalide Tellurium (II) Complexes with Chalcogen Ligands. Synthesis, Spectroscopic Characterization and X-Ray Structural Studies of Bromo[N-methylbenzothialzole-2(3H]-selone] phenyltellurium(II), Bromophenyl[tris(dimethylamino)-phosphaneselenide]tell urium(II) and Tris(dimethylamino) phosphanesulfide
Acta Chem Scand, 9 (759):
[4] A novel polymeric Cd[SSe2N2] central core five-coordinate complex: Synthesis, X-ray structure and 113Cd, 77Se CP MAS NMR characterization of catena(bis(μ2-selenocyanato-N,Se)-(N,N′-dimethylimidazolidine-2-thione-S)-cadmium(II))
Fettouhi, Mohammed
Wazeer, Mohammed I. M.
Isab, Anvarhusein A.
INORGANIC CHEMISTRY COMMUNICATIONS, 2008, 11 (03) : 252 - 255
[5] Synthesis and X-ray structure of the first chloro-bridged thiourea mercury(II) complex [C6H5C(OCH3)NC(S)N(C2H5)2HgCl2]2
Lessmann, F
Beyer, L
Sieler, J
INORGANIC CHEMISTRY COMMUNICATIONS, 2000, 3 (02) : 62 - 64
[6] The first X-ray crystal structure of a mercury(II) complex with an SP(N)3-based ligand: Synthesis and crystal structure of SP(NC5H10)3 and [Hg{SP(NC5H10)3}Cl2]2
Taherzadeh, Maryam
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PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2019, 194 (1-2) : 39 - 46

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