A convenient ultrasonic irradiation technique for in situ synthesis of zinc sulfide nanocrystallites at room temperature

被引：30
|
作者：
Wang, GZ [1 ]
Geng, BY
Huang, XM
Wang, YW
Li, GH
Zhang, LD
机构：
[1] Chinese Acad Sci, Inst Solid State Phys, Hefei 230031, Peoples R China
[2] Hefei Univ Technol, Fac Mat Sci & Engn, Hefei 230009, Peoples R China
来源：
APPLIED PHYSICS A-MATERIALS SCIENCE & PROCESSING | 2003年 / 77卷 / 07期
关键词：
D O I：
10.1007/s00339-002-2033-0
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
Nanocrystalline ZnS has been synthesized using a sonochemical reaction of a mixed solution of Zn(NO3)(2), Na2S2O3 and (CH3)(2)(OH)CH in Ar under ambient conditions. Detailed investigations with X-ray powder diffraction (XRD), transmission electron microscopy (TEM) and X-ray photoelectron spectroscopy (XPS) are reported. It was found that phase-pure ZnS nanocrystallites were produced, and the ZnS nanoparticles were about 6.5 nm in size, as indicated by TEM observation. The chemical mechanism for the formation of ZnS nanocrystals is discussed. This convenient method is found to be an efficient way to produce other chalcogenides as well.
引用
收藏
页码：933 / 936
页数：4
相关论文
共 50 条
  • [1] A convenient ultrasonic irradiation technique for in situ synthesis of zinc sulfide nanocrystallites at room temperature
    G.Z. Wang
    B.Y. Geng
    X.M. Huang
    Y.W. Wang
    G.H. Li
    L.D. Zhang
    Applied Physics A, 2003, 77 : 933 - 936
  • [2] A convenient ultraviolet irradiation technique for in situ synthesis of CdS nanocrystallites at room temperature
    Wang, CY
    Mo, X
    Zhou, Y
    Zhu, YR
    Liu, HT
    Chen, ZY
    JOURNAL OF MATERIALS CHEMISTRY, 2000, 10 (03) : 607 - 608
  • [3] Room temperature synthesis of CdS nanocrystallites
    Bancu, L.
    Meghea, A.
    Simonescu, C.
    Zecheru, T.
    MOLECULAR CRYSTALS AND LIQUID CRYSTALS, 2008, 483 : 237 - 243
  • [4] Influence of ultrasonic irradiation power on the synthesis of ZnS nanocrystallites
    Key Laboratory of Auxiliary Chemistry and Technology for Chemical Industry, Ministry of Education, Shaanxi University of Science and Technology, Xi'an 710021, China
    Kuei Suan Jen Hsueh Pao, 2009, 11 (1843-1846):
  • [5] In situ synthesis and characterization of lead sulfide nanocrystallites in the modified hyperbranched polyester by gamma-ray irradiation
    Zhao, YB
    Zou, JH
    Shi, WF
    MATERIALS SCIENCE AND ENGINEERING B-SOLID STATE MATERIALS FOR ADVANCED TECHNOLOGY, 2005, 121 (1-2): : 20 - 24
  • [6] Room temperature solid-state reaction-a convenient novel route to nanotubes of zinc sulfide
    Zhou, TY
    Xin, XQ
    NANOTECHNOLOGY, 2004, 15 (05) : 534 - 536
  • [7] Synthesis and Room Temperature Magnetic Behavior of Nickel Oxide Nanocrystallites
    Wongsaprom, Kwanruthai
    Maensiri, Santi
    CHIANG MAI JOURNAL OF SCIENCE, 2013, 40 (01): : 99 - 108
  • [8] In situ formation and assembly of CdS nanocrystallites into polyhedrons on Eggshell membrane at room temperature
    Su, Huilan
    Xu, Jia
    Chen, Jianjun
    Moon, Won-Jin
    Zhang, Di
    APPLIED PHYSICS A-MATERIALS SCIENCE & PROCESSING, 2012, 106 (01): : 93 - 97
  • [9] Size-selected zinc sulfide nanocrystallites: Synthesis, structure, and optical studies
    Nanda, J
    Sapra, S
    Sarma, DD
    Chandrasekharan, N
    Hodes, G
    CHEMISTRY OF MATERIALS, 2000, 12 (04) : 1018 - 1024
  • [10] In situ formation and assembly of CdS nanocrystallites into polyhedrons on Eggshell membrane at room temperature
    Huilan Su
    Jia Xu
    Jianjun Chen
    Won-Jin Moon
    Di Zhang
    Applied Physics A, 2012, 106 : 93 - 97
12345