Synthesis and characterization of some fused tricyclic spermidine derivatives of cyclotriphosphazene

被引：5
|
作者：
Ibisoglu, Hanife [1 ]
机构：
[1] Gebze Inst Technol, Dept Chem, TR-41400 Kocaeli, Turkey
来源：
HETEROCYCLES | 2007年 / 71卷 / 10期
关键词：
D O I：
10.1016/S0385-5414(07)81093-8
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A number of derivatives of 6-chloro-2, 2-X-2-1, 3, 5, 7, 11, 16-hexa aza-4,6-diphosphatricyclohexadeca-2, 4, 6-triene {X=SPh, [OCH2(CF2)(2)CH2O](0.5), pyr, NMe2, NHPrn, Ph, NHBut} have been synthesised using two different reaction routes (1, 2) giving rise to penta-substituted-mono-chloro-compounds. The remaining chlorine atom in these products was reluctant to react with neutral nitrogen nucleophiles. The structures of the compounds were determined by elemental analysis, mass spectrometry and by H-1 and P-31-NMR spectrocsopy.
引用
收藏
页码：2173 / 2181
页数：9
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