DETERMINATION OF STEROID HORMONES IN SOMES RIVER WATER BY SOLID PHASE MICROEXTRACTION AND GAS CHROMATOGRAPHY-MASS SPECTROMETRY

被引：0
|
作者：
Senila, Lacrimioara [1 ]
Miclean, Mirela [1 ]
Roman, Cecilia [1 ]
Majdik, Cornelia [2 ]
Zaray, Gyula [3 ]
机构：
[1] Res Inst Analyt Instrumentat, INCDO INOE 2000, Cluj Napoca 400293, Romania
[2] Univ Babes Bolyai, Fac Chem & Chem Engn, Cluj Napoca 400028, Romania
[3] Eotvos Lorand Univ, Dept Analyt Chem, Inst Chem, Budapest, Hungary
来源：
STUDIA UNIVERSITATIS BABES-BOLYAI CHEMIA | 2009年 / 54卷 / 04期
关键词：
steroid hormones; SPME; MSTFA; GC-MS; ENDOCRINE-DISRUPTING CHEMICALS; DERIVATIZATION;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
In this study, the occurrence of steroid hormones in Somes River was evaluated. The water samples were collected downstream of municipal sewage treatment plant of Cluj-Napoca, Romania. The used method was based on solid-phase microextraction (SPME), on-fiber silylation and, final, analysis by gas chromatography-mass spectrometry (GC-MS). The target compounds were estrone and beta-estradiol and were detected in wastewater effluent and river water. The values of target compounds in water samples were in the range of 0.010-0.080 mu g/l.
引用
收藏
页码：179 / 186
页数：8
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