Synthesis and characteristic of carbon-encapsulated ferronickel nanoparticles by detonation decomposition of doping with nitrate explosive precursors

被引:26
|
作者
Luo Ning [1 ]
Li Xiaojie [1 ]
Sun Yuling [2 ]
Wang Xiaohong [1 ]
机构
[1] Dalian Univ Technol, State Key Lab Struct Anal Ind Equipment, Dalian 116024, Peoples R China
[2] Artillery Acad PLA, Hefei 230031, Peoples R China
基金
美国国家科学基金会;
关键词
Composite nanoparticles; Nanostructure; Detonation synthesis; Transmission electron microscopy; Magnetic properties; MAGNETIC-PROPERTIES; IRON NANOPARTICLES; NI NANOPARTICLES; COATED COBALT; ARC-DISCHARGE; NANOCAPSULES; FE; CO;
D O I
10.1016/j.jallcom.2010.05.181
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Synthesizing carbon-encapsulated ferronickel nanoparticles was developed by a detonation method. The composite precursors were ignited in the nitrogen in closed explosion vessel. These composite nanoparticles were characterized with transmission electron microscope, energy-dispersive X-ray spectrometer, X-ray diffraction, X-ray fluorescence, Raman spectroscopy and magnetic measurement. Results indicated that carbon-encapsulated ferronickel nanoparticles with diameters ranging from 10 to 50 nm were produced and the composite nanoparticles were with a core-shell structure. The composite nanoparticles were synthesized with the yield about 10-15% one time. (C) 2010 Elsevier B.V. All rights reserved.
引用
收藏
页码:352 / 356
页数:5
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