Hydrothermal synthesis, characterization and thermal behavior of a new zirconium phosphate fluoride

被引：0
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作者：
Sun, Z [1 ]
Liu, Z
Xu, L
Yang, Y
He, Y
机构：
[1] Chinese Acad Sci, Dalian Inst Chem Phys, Dept Nat Gas Chem & Appl Catalysis, Dalian 116023, Peoples R China
[2] Liaoning Normal Univ, Dept Chem, Dalian 116029, Peoples R China
来源：
RECENT ADVANCES IN THE SCIENCE AND TECHNOLOGY OF ZEOLITES AND RELATED MATERIALS, PTS A - C | 2004年 / 154卷
关键词：
zirconium phosphate; hydrotherinal synthesis; P-31 MAS NMR;
D O I：
暂无
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
A new organically templated zirconium phosphate fluoride (denoted here ZrPO4-8) has been synthesized hydrothermally in a reactant system of ZrOCl2-en-NH4F-H-3PO4-H2O by using NH4F as the mineralizer. Based oil X-ray powder diffraction (XRD), X-ray fluorescence analysis (XRF), IR spectroscopy, scanning electron microscope (SEM), TG-DTA analysis and P-31 MAS NMR spectroscopy, the as-synthesized product is assigned to be a novel compound. The thermal behavior of the title compound has been investigated by using X-ray thermodiffractometry and TG-DTA analysis.
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页码：1056 / 1059
页数：4
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