Synthesis and Characterization of Fe-FeOx Core-Shell Nanowires

被引:12
|
作者
Lee, Ju Hun [1 ]
Wu, Jun Hua [2 ]
Lee, Ji Sung [1 ]
Jeon, Ki Seok [3 ]
Kim, Hae Ryong [1 ]
Lee, Jong Heun [1 ]
Suh, Yung Doug [3 ]
Kim, Young Keun [1 ]
机构
[1] Korea Univ, Dept Mat Sci & Engn, Seoul 136713, South Korea
[2] Korea Univ, Res Inst Engn & Technol, Seoul 136713, South Korea
[3] Korea Res Inst Chem Technol, Fus Biotechnol Res Ctr, Taejon 305343, South Korea
关键词
Core-shell nanowires; iron; iron oxide; nano-Raman; nanostructure;
D O I
10.1109/TMAG.2008.2001515
中图分类号
TM [电工技术]; TN [电子技术、通信技术];
学科分类号
0808 ; 0809 ;
摘要
We report the synthesis and characterization of Fe - FeOx core-shell nanowires by thermal conversion of the Fe nanowires from pulse electrodeposition in anodized aluminum oxide (AAO) nanotemplates under various conditions. Well-defined core-shell nanostructure of the Fe - FeOx nanowires was confirmed by TEM and corresponding elemental line scanning and point scanning. The type of the iron oxide in the shell was identified using nano-Raman spectroscopy, which exposes magnetite to be the major constituent. The magnetic measurements demonstrate that the nanowires are robustly soft magnetic, with the magnetization tunable by heat treatment parameters and a weak magnetic easy direction parallel to the nanowire axis.
引用
收藏
页码:3950 / 3953
页数:4
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