(E)-Ethyl 3-(3,4-dihydroxyphenyl)prop-2-enoate: a natural polymorph extracted from Aristotelia chilensis (Maqui)

被引：0
|
作者：
Paz, Cristian [1 ]
Moreno, Yanko [2 ]
Becerra, Jose [1 ]
Silva, Mario [1 ]
Burgos, Viviana [1 ]
Freire, Eleonora [3 ,4 ]
Baggio, Ricardo [3 ]
机构：
[1] Univ Concepcion, Fac Ciencias Nat & Oceanog, Lab Quim Prod Nat, Concepcion, Chile
[2] Univ Concepcion, Fac Ciencias Quim, Dept Quim Analit & Inorgan, Concepcion, Chile
[3] Comis Nacl Energia Atom, Ctr Atom Constituyentes, RA-1429 Buenos Aires, DF, Argentina
[4] Univ Nacl Gen San Martin, Escuela Ciencia & Tecnol, Buenos Aires, DF, Argentina
来源：
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY | 2013年 / 69卷
关键词：
D O I：
10.1107/S0108270113013991
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The natural title compound, C11H12O4, extracted from the Chilean native tree Aristotelia chilensis (Maqui), is a polymorph of the synthetic E form reported by Xia, Hu & Rao [Acta Cryst. (2004), E60, o913-o914]. Both rotational conformers are identical from a metrical point of view, and only differ in the orientation of the 3,4-dihydroxyphenyl ring with respect to the rest of the molecule, which leads to completely different crystal structure arrangements and packing efficiencies. The reasons behind both reside in the different hydrogen-bonding interactions.
引用
收藏
页码：765 / +
页数：10
相关论文
共 50 条
  • [1] Propyl 3-(3,4-dihydroxyphenyl)prop-2-enoate
    Xia, Chun-Nian
    Hu, Wei-Xiao
    Zhou, Wei
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O2482 - U913
  • [2] Butyl 3-(3,4-dihydroxyphenyl)prop-2-enoate
    Xia, CN
    Hu, WX
    Zhou, W
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O1112 - O1113
  • [3] Octyl 3-(3,4-dihydroxyphenyl)prop-2-enoate
    Xia, Chun-Nian
    Hu, Wei-Xiao
    Zhou, Wei
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O3900 - O3901
  • [4] tert-butyl 3-(3,4-dihydroxyphenyl)prop-2-enoate
    Xia, Chun-Nian
    Hu, Wei-Xiao
    Zhou, Wei
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O4118 - O4119
  • [5] Prop-2-ynyl 3-(3,4-dihydroxyphenyl)-prop-2-enoate monohydrate
    Xia, CN
    Zhou, W
    Hu, WX
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O1783 - O1784
  • [6] 2-Methyl-2-nitropropyl 3-(3,4-dihydroxyphenyl)-prop-2-enoate
    Xia, CN
    Hu, WX
    Zhou, W
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O3757 - O3758
  • [7] Ethyl (E)-3-(anthracen-9-yl)prop-2-enoate
    Bugenhagen, Bernhard
    Al Jasem, Yosef
    al Hindawi, Bassam
    Al Rawashdeh, Nathir
    Thiemann, Thies
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O130 - +
  • [8] Ethyl 3-(3,4-dihydroxyphenyl)-2-propenoate
    Xia, CN
    Hu, WX
    Rao, GW
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2004, 60 : O913 - O914
  • [9] Bioactivities of caffeic acid methyl ester (methyl-(E)-3-(3,4-dihydroxyphenyl)prop-2-enoate): a hydroxycinnamic acid derivative from Solanum melongena L. fruits
    P. Usha Rani
    P. Devanand
    Journal of Pest Science, 2013, 86 : 579 - 589
  • [10] Bioactivities of caffeic acid methyl ester (methyl-(E)-3-(3,4-dihydroxyphenyl)prop-2-enoate): a hydroxycinnamic acid derivative from Solanum melongena L. fruits
    Rani, P. Usha
    Devanand, P.
    JOURNAL OF PEST SCIENCE, 2013, 86 (03) : 579 - 589
12345