CONCISE SYNTHESIS OF XIMENYNIC ACID

被引：3
|
作者：
Wang, Lutai [1 ]
Li, Jiabin [2 ]
Xue, Xiaowen [1 ]
机构：
[1] China Pharmaceut Univ, Dept Med Chem, Nanjing 210009, Peoples R China
[2] China Pharmaceut Univ, Dept Inorgan Chem, Nanjing 210009, Peoples R China
来源：
SYNTHETIC COMMUNICATIONS | 2012年 / 42卷 / 23期
关键词：
Chlorination; synthesis; ximenynic acid; SEED OIL;
D O I：
10.1080/00397911.2011.585443
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
An improved synthesis of ximenynic acid (1) starting from castor oil has been developed with the direct chlorination of ricinstearolic acid as the key step. By this modification, the synthetic route was more concise and economic. The separation of geometric somers was achieved by repeated urea fractionation. Supplemental materials are available for this article. Go the publisher's online edition of Synthetic Communications to view the free supplemental file.
引用
收藏
页码：3540 / 3543
页数：4
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