Synthesis of inulin esters of phenylcarboxylic acids

被引：7
|
作者：
Torlopov, M. A. [1 ]
Udoratina, E. V. [1 ]
Kuchin, A. V. [1 ]
机构：
[1] Russian Acad Sci, Ural Branch, Komi Sci Ctr, Inst Chem, Syktyvkar 16798, Russia
来源：
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY | 2013年 / 49卷 / 05期
关键词：
ANTIOXIDANT PROPERTIES; FERULIC ACID;
D O I：
10.1134/S1070428013050114
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Inulin esters were synthesized containing residues of ferulic, p-hydroxycinnamic, and vanillic acids with a maximum degree of substitution of 1.1. The inulin acylation was carried out with chlorides of 4-acetoxy derivatives of the corresponding hydroxyphenylcarboxylic acids in a heterogenic water-organic environment. The removal of the protecting acetyl group at the phenol hydroxyl was carried out by treating with pyrrolidine or ammonium acetate. The solubility of the esters obtained was evaluated.
引用
收藏
页码：702 / 706
页数：5
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