A single-source route to CdS nanorods

被引：78
|
作者：
Nair, PS
Radhakrishnan, T
Revaprasadu, N
Kolawole, GA
O'Brien, P
机构：
[1] Univ Zululand, Dept Chem, ZA-3886 Kwa Dlangezwa, South Africa
[2] Univ Manchester, Dept Chem, Manchester M13 9PL, Lancs, England
[3] Univ Manchester, Manchester Mat Sci Ctr, Manchester M13 9PL, Lancs, England
来源：
CHEMICAL COMMUNICATIONS | 2002年 / 06期
关键词：
D O I：
10.1039/b200434h
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
We report the preparation of CdS nanorods using a thiosemicarbazide complex of cadmium [Cd(NH2CSNHNH2)(2)Cl-2]. The precursor was decomposed in tri-n-octylphosphine oxide (TOPO) at 280 degreesC to give TOPO capped CdS nanoparticles; nano-dimensional rods of the material are clearly visible in transmission electron microscopy (TEM); the particles have been further characterised by X-ray diffraction (XRD) and selected area electron diffraction (SAED) and optical measurements.
引用
收藏
页码：564 / 565
页数：2
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