Synthesis and characterization of β-cyclodextrin modified hyperbranched carbosilane as stationary phase for GC

被引：3
|
作者：
Chen, Guo Wen [1 ,2 ]
Zhang, Chen [1 ]
Li, Wen Jie [1 ]
Zhou, Chuan Jian [1 ]
Feng, Sheng Yu [2 ]
机构：
[1] Shandong Univ, Sch Mat Sci & Engn, Jinan 250061, Peoples R China
[2] Minist Educ China, Key Lab Special Funct Aggregated Mat, Jinan 250100, Peoples R China
来源：
CHINESE CHEMICAL LETTERS | 2012年 / 23卷 / 11期
基金：
中国国家自然科学基金;
关键词：
Hyperbranched carbosilane; Cyclodextrin; Stationary phase; Gas chromatography; GAS-CHROMATOGRAPHY; LIQUID-CHROMATOGRAPHY; SEPARATION;
D O I：
10.1016/j.cclet.2012.09.012
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A new beta-cyclodextrin modified hyperbranched carbosilane stationary phase for gas chromatography was synthesized by substituting the -OH groups of beta-cyclodextrin with hyperbranched carbosilane and was coated on the inner wall of fused silica capillary column for gas chromatography. The chromatographic behaviors of the stationary phase were studied. The initial testing results showed that it possessed good separation abilities for several kinds of mixtures, such as benzenes, acrylates, ketones and alkylchlorides. (C) 2012 Chuan Jian Zhou. Published by Elsevier B.V. on behalf of Chinese Chemical Society. All rights reserved.
引用
收藏
页码：1259 / 1262
页数：4
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