Highly Efficient One-Pot Three-Component Synthesis of Naphthopyran Derivatives in Water Catalyzed by Phosphates

被引：38

作者：

Essamlali, Younes ^{[1
,3
]}

Amadine, Othmane ^{[1
,3
]}

Maati, Houda ^{[1
,3
]}

Abdelouahdi, Karima ^{[2
]}

Fihri, Aziz ^{[1
]}

Zahouily, Mohamed ^{[1
,3
]}

Varma, Rajender S. ^{[4
]}

Solhy, Abderrahim ^{[1
]}

机构：

[1] MAScIR Fdn, INANOTECH, VARENA Ctr, Rabat 10100, Morocco

[2] CNRST, Div UATRS, Angle Allal Fassi FAR, Rabat 10000, Morocco

[3] Univ Hassan II Mohammedia, Fac Sci & Tech, URAC 24, Lab Mat Catalyse & Valorisat Ressources Nat, Mohammadia 20650, Morocco

[4] US EPA, Natl Risk Management Res Lab, Sustainable Technol Div, Cincinnati, OH 45268 USA

来源：

ACS SUSTAINABLE CHEMISTRY & ENGINEERING | 2013年 / 1卷 / 09期

关键词：

Three-component reactions; One-pot method; Heterogeneous catalysis; Phosphates; Sustainable chemistry; AQUA MEDIATED SYNTHESIS; ONE-STEP SYNTHESIS; SUBSTITUTED; 2-AMINO-4H-CHROMENES; MULTICOMPONENT REACTIONS; MODIFIED-HYDROXYAPATITE; SOLID CATALYST; CONVENIENT; 2-AMINO-2-CHROMENES; COMBINATORIAL; INHIBITORS;

D O I：

10.1021/sc400072s

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

An expeditious and efficient protocol for the synthesis of naphthopyrans has been developed that proceeds via a one-pot three-component sequential reaction in water catalyzed by phosphates (hydroxyapatite or sodium-modified hydroxyapatite). This is part of the mission to maximize valorization efforts of Moroccan natural phosphate resources. The title compounds have been obtained in high yield and purity. The catalyst can be reused several times, making this procedure facile, practical, and sustainable.

引用

页码：1154 / 1159

页数：6

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