Simultaneous measurements of X-ray diffraction (XRD) and differential scanning calorimetry (DSC) data under controlled humidity condition: Instrumentation and application to studies on hydration, dehydration, and rehydration processes of pharmaceutical compounds

被引:7
|
作者
Kishi, A [1 ]
Toraya, H [1 ]
机构
[1] Rigaku Corp, Tokyo 1968666, Japan
关键词
D O I
10.1154/1.1649321
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
An instrument for the simultaneous measurement of X-ray powder diffraction (XRD) data and differential scanning calorimetry (DSC) data under a controlled humidity condition has been developed in order to achieve a design concept of reliable and simple in operation. Examples of the application to studies on hydration, dehydration, and rehydration processes of pharmaceutical compounds under various humidity conditions are presented. The usefulness of the present XRD-DSC system will be demonstrated. (C) 2004 International Centre for Diffraction Data.
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页码:31 / 35
页数:5
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