Mechanosynthesis of nanocrystalline Cu with Al2O3 dispersion by cryogenic milling

被引:0
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作者
Lee, Jin-Hyung [1 ]
Hwang, Seung J. [1 ]
机构
[1] Daejin Univ, Dept Mat Sci & Engn, Pochon 487711, Kyung Gi, South Korea
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中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Nanocrystalline Cu with Al2O3 dispersoid (Cu-4.1 vol.% Al2O3) was successfully produced by a simple cryo-milling at 210K with a mixture of Cu2O, Al, and Cu powders, followed by hot pressing at 1123K. The results of microstructural analysis showed that the hot pressed materials comprised a mixture of Cu matrix (25.1 nm) and Al2O3 (<10 nm) with a homogeneous size distribution of the dispersoid. Grain sizes of Cu were estimated by XRD (Scherrer's formula) and TEM; dispersoid sizes of Al2O3 were confirmed by STEM-EDS (Scanning Transmission Electron Microscopy-Energy Dispersive Spectroscopy) and TEM (Transmission Electron Microscopy).
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页码:289 / 292
页数:4
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