Crystal structure of 2-(2-bromophenyl)-5-ethyl-1,3-dioxane-5-carboxylic acid, C13H15BrO4

被引：0
|
作者：
Yuan, Lin [2 ]
Yuan, Xian-You [2 ]
Li, Zhong-Yan [2 ]
Zhang, Min [1 ,2 ]
机构：
[1] Hunan Univ Sci & Engn, Key Lab Comprehens Utilizat Adv Plants Resources, Yongzhou 425199, Hunan, Peoples R China
[2] Hunan Univ Sci & Engn, Coll Chem & Bioengn, Yongzhou 425199, Hunan, Peoples R China
来源：
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES | 2016年 / 231卷 / 04期
关键词：
CLEAVABLE SURFACTANTS; 1,3-DIOXANE RING;
D O I：
10.1515/ncrs-2016-0136
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
C13H15BrO4, orthorhombic, Pbca (no. 61), a = 15.894(3) angstrom, b = 7.6064(16) angstrom, c = 21.571(4) angstrom, V = 2607.8(9) angstrom(3), Z = 8, R-gt(F) = 0.0268, wR(ref)(F-2) = 0.0702, T = 296(2) K. CCDC no.: 1500923 The asymmetric unit of the tilte crystal structure is shown in the figure. Tables 1 and 2 contain details of the measurement method and a list of the atoms including atomic coordinates and displacement parameters.
引用
收藏
页码：1209 / 1210
页数：2
相关论文
共 50 条
  • [1] Crystal structure of 2-(4-Bromophenyl)-5-ethyl-1,3-dioxane-5-carboxylic acid, C13H15BrO4
    Jia, Guo-Kai
    Yuan, Lin
    Zhang, Min
    Yuan, Xian-You
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2016, 231 (03): : 959 - 960
  • [2] Crystal structure of 2-(2-bromophenyl)-5-methyl-1,3-dioxane-5-carboxylic acid, C12H13BrO4
    Jia, Guo-Kai
    Yuan, Lin
    Zhang, Min
    Yuan, Xian-You
    Liu, Fang
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2016, 231 (04): : 1207 - 1208
  • [3] Crystal structure of (2-(4-bromophenyl)-5-ethyl-1,3-dioxan-5-yl)methanol, C13H17BrO3
    Zhang, Xing-Yu
    Yuan, Lin
    Zhang, Min
    Yuan, Xian-You
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2016, 231 (03): : 961 - 963
  • [4] Crystal structure of 2-(4-chlorophenyl)-5-methyl-1,3-dioxane-5-carboxylic acid, C12H13ClO4
    Zhang, Min
    Jia, Guo-Kai
    Yuan, Lin
    Yuan, Xian-You
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2013, 228 (03): : 393 - 394
  • [5] Crystal structure of (Z)-2-(1-bromo-2-phenylvinyl)-5-ethyl-2-methyl-1,3-dioxane-5-carboxylic acid, C15H17Br1O4
    Jia, Guo-Kai
    Yuan, Xian-You
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2022, 237 (04): : 661 - 662
  • [6] Crystal structure of 5-methyl-2-phenyl-1,3-dioxane-5-carboxylic acid, C12H14O4
    Yuan, Xian-You
    Jia, Guo-Kai
    Zhang, Min
    Yuan, Lin
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2016, 231 (01): : 5 - 7
  • [7] 2-(2-Chlorophenyl)-5-methyl-1,3-dioxane-5-carboxylic acid
    Jia, Guo-Kai
    Yuan, Lin
    Zhang, Min
    Yuan, Xian-You
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O2037 - +
  • [8] Crystal structure of 5-ethyl-2-(p-tolyl)-1,3-dioxane-5-carboxylic acid, C14H18O4
    Jia, Guo-Kai
    Yuan, Lin
    Yuan, Xian-You
    Li, Zhong-Yan
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2017, 232 (05): : 819 - 820
  • [9] Crystal structure of 2-(2-hydroxy-5-nitrophenyl)-5-methyl-1,3-dioxane-5-carboxylic acid, C12H13N1O7
    Jia, Guo-Kai
    Yuan, Xian-You
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2022, 237 (04): : 693 - 694
  • [10] Syntheses and crystal structures of 2,2,5-trimethyl-1,3-dioxane-5-carboxylic acid and 2,2,5-trimethyl-1,3-dioxane-5-carboxylic anhydride
    Giesen, Joseph A.
    Grayson, Scott M.
    Mague, Joel J.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2020, 76 : 86 - +
12345