Synthesis and characterization of α-{3-[2-hydroxy-3-(N-methyl-N-hydroxy-ethylamino)propoxy]propyl}-ω-butylpolydimethylsiloxanes

被引:2
|
作者
Sun, Hai Feng [1 ]
Zhang, Qing Si [1 ]
Zhang, Meng [2 ]
Yu, Yi Tao [1 ]
Zong, Jian Ping [1 ]
机构
[1] Shandong Inst Light Ind, Sch Chem Engn, Jinan 250100, Peoples R China
[2] Jiangnan Univ, Sch Chem & Mat, Wuxi 214122, Peoples R China
关键词
Anionic ring-opening polymerization; Hydrosilylation; Epoxy addition; alpha-{3-[2-Hydroxy-3-(N-methyl-N-hydroxyethylamino)propoxy]propyl}-omega-butylpolydimethylsiloxanes;
D O I
10.1016/j.cclet.2008.06.047
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
alpha-{3-[2-hydroxy-3-(N-methyl-N-hydroxyethylamino)propoxy]propyl}-omega-butylpolydimethylsiloxanes III with various molecular weights were prepared by epoxy addition of alpha-[3-(2,3-epoxy-propoxy)propyl]-omega-butylpolydimethylsiloxanes II and N-methylmonoethanolamine. At each step, the outcome compounds were characterized through FT-IR and NMR spectra, the results showed that each step was successfully carried out and objective products were achieved. (C) 2008 Qing Si Zhang. Published by Elsevier B. V. on behalf of Chinese Chemical Society. All rights reserved.
引用
收藏
页码:1196 / 1198
页数:3
相关论文
共 50 条
  • [1] Synthesis and characterization ofα-{ 3-[2-hydroxy-3-(N-methyl-N-hydroxy-ethylamino)propoxy]propyl}-ω-butylpolydimethylsiloxanes
    Hai Feng Sun~a Qing Si Zhang~(a
    Chinese Chemical Letters, 2008, (10) : 1196 - 1198
  • [2] Synthesis and Characterization of α-Butyl-omega-{3-[2-hydroxy-3-(N-methyl-n-hydroxyethylamino)propoxy]propyl}polydimethylsiloxane
    Sun, Haifeng
    Zhang, Qingsi
    Zhang, Meng
    Yu, Yitao
    Zong, Jianping
    JOURNAL OF APPLIED POLYMER SCIENCE, 2010, 117 (02) : 882 - 887
  • [4] Synthesis and characterization of α-{3-[(2,3-dihydroxy)propoxy]propyl}-ω-butylpolydimethylsiloxanes
    Zhan, Xiao Li
    Luo, Zhen Huan
    Zhang, Qing Hua
    Chen, Bi
    Chen, Feng Qiu
    CHINESE CHEMICAL LETTERS, 2009, 20 (06) : 729 - 732
  • [5] Synthesis of N-[2-Hydroxy-3-(vinyloxy)propyl]- and N-{2-Hydroxy-3-[2-(vinyloxy)ethoxy]propyl}-imidazolidin-2-ones
    Kukharev, B. F.
    Stankevich, V. K.
    Lobanova, N. A.
    Stankevich, V. V.
    Bragin, E. V.
    Volkov, G. A.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2010, 46 (08) : 1264 - 1265
  • [6] Synthesis of N-[2-hydroxy-3-(vinyloxy)propyl]- and N-{2-hydroxy-3-[2-(vinyloxy)ethoxy]propyl}-imidazolidin-2-ones
    B. F. Kukharev
    V. K. Stankevich
    N. A. Lobanova
    V. V. Stankevich
    E. V. Bragin
    G. A. Volkov
    Russian Journal of Organic Chemistry, 2010, 46 : 1264 - 1265
  • [7] Copolymers of 2-hydroxy-3-( N-methyl- N-phenylamino)propyl methacrylate with methyl methacrylate and their microstructure
    Gaysin, Adel I.
    Vakhonina, Tatyana A.
    Yakovleva, Ekaterina O.
    Balakina, Marina Yu.
    Sinyashin, Oleg G.
    MENDELEEV COMMUNICATIONS, 2024, 34 (03) : 332 - 334
  • [8] STRUCTURE OF PROPYL 3-ACETYL-4-[2-HYDROXY-3-(ISOPROPYLAMINO)PROPOXY]CARBANILATE HYDROCHLORIDE
    KETTMANN, V
    CSOLLEI, J
    JECNY, J
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 1992, 48 : 292 - 295
  • [9] 3-[2-Hydroxy-3-(2,4,6-trimethylphenyl)propyl]-3-methyl-1-phenylthiourea
    Maharramov, Abel M.
    Khalilov, Ali N.
    Sadikhova, Nurlana D.
    Gurbanov, Atash V.
    Ng, Seik Weng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O1087 - U1893
  • [10] Synthesis, characterization and kinetic study of photocrosslinkable prepolymer: 2-hydroxy-3-[p-(1-{p-[2-hydroxy-3-(vinylcarbonyloxy)propoxy]phenol}-1-phenylethyl)phenoxy]propyl acrylate
    Kumar, D.
    Jaikumar, V.
    DESIGNED MONOMERS AND POLYMERS, 2015, 18 (03) : 295 - 302