Synthesis and crystal structure of PdSnTe

被引：2
|
作者：
Laufek, F. [1 ]
Vymazalova, A. [1 ]
Navratil, J. [2 ,3 ]
Drabek, M. [1 ]
Plasil, K. [4 ]
Plechacek, T. [2 ,3 ]
机构：
[1] Czech Geol Survey, Prague 15200 5, Czech Republic
[2] Joint Lab Solid State Chem IMC AS CR, Pardubice 53210, Czech Republic
[3] Univ Pardubice, Pardubice 53210, Czech Republic
[4] Charles Univ Prague, Fac Sci, Prague 12843 2, Czech Republic
来源：
JOURNAL OF ALLOYS AND COMPOUNDS | 2009年 / 468卷 / 1-2期
关键词：
PdSnTe; Crystal structure; X-ray powder diffraction; Electrical conductivity;
D O I：
10.1016/j.jallcom.2008.01.065
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
The compound with composition PdSnTe was prepared by heating of stoichiometric amount of Pd, Sn and Te in silica glass tube at 400 C. Its crystal structure was refined by Rietveld method using conventional X-ray powder diffraction data. PdSnTe shows orthorhombic symmetry, space group Pbca with unit cell parameters a = 6.5687(2), b = 6.6029(2), c = 12.9949(4) A, V = 558.8(1) A(3) and Z= 8. The title compound can be viewed its a ternary-ordered variant of alpha-NiAs(2)-type structure, it is isostructural with PtSiTe. Temperature dependence of electrical Conductivity and Hall coefficient are presented, it suggests semimetallic or strongly degenerated semiconductor behaviour of the prepared compound. (c) 2008 Elsevier B.V. All rights reserved.
引用
收藏
页码：69 / 72
页数：4
相关论文
共 50 条
  • [1] Synthesis and crystal structure of azafulgides
    WANG Fan
    WANG Huan-Zhong*
    LI Yun-Zheng
    FAN Guang-Yu
    CUI Xiu-Shan
    LIU Zuo-Cai
    Acta Chimica Sinica(English Edition), 1989, (04) : 349 - 355
  • [2] Synthesis and crystal structure of β-hexanitrohexaazaisowurtzitane
    欧育湘
    贾会平
    徐永江
    陈博仁
    范广裕
    刘利华
    郑福平
    潘则林
    王才
    Science in China(Series B), 1999, (02) : 217 - 224
  • [3] Synthesis and crystal structure of diferrocenylmethoxyethylamine
    Zhang, Haibo
    Li, Baoguo
    Hu, Ruijue
    Bian, Zhanxi
    Bai, Shuzhen
    STRUCTURAL CHEMISTRY, 2006, 17 (05) : 477 - 481
  • [4] Synthesis and crystal structure of tristropocryptands
    Shindo, K
    Wakabayashi, H
    Kurihara, T
    Zhang, LC
    JOURNAL OF THE CHINESE CHEMICAL SOCIETY, 2003, 50 (01) : 47 - 50
  • [5] Synthesis and crystal structure of β-hexanitrohexaazaisowurtzitane
    Yuxiang Ou
    Huiping Jia
    Yongjiang Xu
    Boren Chen
    Guangyu Fan
    Lihua Liu
    Fuping Zheng
    Zelin Pan
    Cai Wang
    Science in China Series B: Chemistry, 1999, 42 : 217 - 224
  • [6] Synthesis and Crystal Structure of Carvedilol
    CHEN Wei-Min
    XU Ji-Hong ( Institute of Pharmaceutical Sciences
    ZENG Long-Mei
    ( Department of Chemistry
    YU Kai-Bei
    ( Chengdu Institue of Analysis
    结构化学, 1998, (05) : 325 - 328
  • [7] Synthesis and crystal structure of pilloin
    Yang, Hong-Bing
    Wang, Yan-Chang
    Zhang, Zun-Ting
    Chang, Yong
    TURKISH JOURNAL OF CHEMISTRY, 2008, 32 (01) : 87 - 95
  • [8] Synthesis and crystal structure of β-hexanitrohexaazaisowurtzitane
    Ou, YX
    Jia, HP
    Xu, YJ
    Chen, BR
    Fan, GY
    Liu, LH
    Zheng, FP
    Pan, ZL
    Wang, C
    SCIENCE IN CHINA SERIES B-CHEMISTRY, 1999, 42 (02): : 217 - 224
  • [9] Synthesis and Crystal Structure of a Thiosemicarbazone
    Li, Peiyuan
    Su, Wei
    Lu, Chengsheng
    Liu, Lifeng
    Zhou, Quan
    Qian, Quanquan
    ASIAN JOURNAL OF CHEMISTRY, 2013, 25 (14) : 8213 - 8214
  • [10] Synthesis and crystal structure of diferrocenylmethoxyethylamine
    Haibo Zhang
    Baoguo Li
    Ruijue Hu
    Zhanxi Bian
    Shuzhen Bai
    Structural Chemistry, 2006, 17 : 477 - 481
12345