Investigation of the Ordering of Porous Anodic Alumina Formed by Anodization of Aluminum in Selenic Acid

被引：15

作者：

Nazarkina, Yulia ^{[1
]}

Gavrilov, Sergei ^{[1
]}

Terryn, Herman ^{[2
]}

Petrova, Manuela ^{[2
]}

Ustarroz, Jon ^{[2
]}

机构：

[1] Natl Res Univ Elect Technol MIET, Dept Mat Funct Elect MFE, Moscow 124498, Russia

[2] Vrije Univ Brussel, SURF, Res Grp Electrochem & Surface Engn, B-1050 Brussels, Belgium

来源：

JOURNAL OF THE ELECTROCHEMICAL SOCIETY | 2015年 / 162卷 / 09期

关键词：

LOCAL BURNING PHENOMENA; OXALIC-ACID; INTERPORE DISTANCE; RAMAN-SPECTRA; PORE ARRAYS; OXIDE; TEMPERATURE; GROWTH; LUMINESCENCE; FABRICATION;

D O I：

10.1149/2.0571509jes

中图分类号：

O646 [电化学、电解、磁化学];

学科分类号：

081704 ;

摘要：

The formation of porous alumina by galvanostatic anodization in selenic acid has been investigated. The influence of the electrolyte concentration on the morphological features and the self-ordering behavior of the porous oxide film has been studied. The best pore arrangement is obtained upon anodization in 0.5 M H2SeO4. Using chronopotentiometry, gravimetric analysis and FESEM it is shown that the highest degree of pore ordering is caused by an optimal combination of the two mechanisms that lead to pore initiation: mechanical instability and field-assisted dissolution. In addition, by means of Raman spectroscopy it is found that the optical properties of porous alumina anodized in selenic acid do not exhibit parasite effects due to electrolyte incorporation during anodization. Hence, these templates are of great interest to fabricate and investigate functional nanostructures for optoelectronics. (C) 2015 The Electrochemical Society. All rights reserved.

引用

页码：E166 / E172

页数：7

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