Synthesis and characterization of strontium titanate powder via a simple polymer solution route

被引:0
|
作者
Lee, Sang-Jin [2 ]
Thiyagarajan, Pradheep [1 ]
Lee, Man-Jong [1 ]
机构
[1] Konkuk Univ, Dept Adv Technol Fus, Seoul 143701, South Korea
[2] Mokpo Natl Univ, Dept Adv Mat Sci & Engn, Muan 534729, South Korea
来源
关键词
strontium titanate; titanium isopropoxide; strontium nitrate; ethylene glycol; powder synthesis; complexation-polymerization;
D O I
暂无
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
A simple chemical route has been used to synthesize highly sinterable strontium titanate (SrTiO3) powders using titanium isopropoxide, strontium nitrate and ethylene glycol. This method utilizes complexation-polymerization using ethylene glycol as an organic carrier, which leads to compositional homogeneity and fine particle sizes. The calcined SrTiO3 powder showing a porous nature was fully crystallized to a cubic phase at 1,300 degrees C for 1 hour. Through ball-milling the porous SrTiO3 powders with particle sizes of 200-300 nm were easily obtained, which was sintered to a bulk density of 4.8 g/cm(3) at 1,400 degrees C for 1 h with a grain size of approximately 6.0 mm. The relative dielectric constant and loss tangent of SrTiO3 sintered at 1,400 degrees C for 1 hour were 2078 and 0.022, respectively
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页码:385 / 388
页数:4
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