Modulated synthesis of zirconium-metal organic framework (Zr-MOF) for hydrogen storage applications

被引：152
|
作者：
Ren, Jianwei [1 ]
Langmi, Henrietta W. [1 ]
North, Brian C. [1 ]
Mathe, Mkhulu [1 ]
Bessarabov, Dmitri [2 ]
机构：
[1] CSIR, HySA Infrastruct Ctr Competence Mat Sci & Mfg, ZA-0001 Pretoria, South Africa
[2] NWU, Fac Engn, HySA Infrastruct Ctr Competence, ZA-2520 Potchefstroom, South Africa
来源：
INTERNATIONAL JOURNAL OF HYDROGEN ENERGY | 2014年 / 39卷 / 02期
关键词：
Zirconium-metal organic framework; Modulated synthesis; Hydrogen storage; Nucleation rate; DETERMINING SURFACE-AREAS; BET METHOD; ADSORPTION; DESIGN;
D O I：
10.1016/j.ijhydene.2013.10.087
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
A modulated synthesis of Zr-metal organic framework (Zr-MOF) with improved ease of handling and decreased reaction time is reported to yield highly crystalline Zr-MOF with well-defined octahedral shaped crystals for practical hydrogen storage applications. The Zr-MOF obtained from the modulated synthesis showed high thermal and moisture stabilities with enhanced hydrogen storage capacity. Further study suggests that the modulated synthesis of Zr-MOF may lead to the development of a flow-through synthesis process. Copyright (C) 2013, Hydrogen Energy Publications, LLC. Published by Elsevier Ltd. All rights reserved.
引用
收藏
页码：890 / 895
页数：6
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