Screening of Anthocyanins and Anthocyanin-Derived Pigments in Red Wine Grape Pomace Using LC-DAD/MS and MALDI-TOF Techniques

被引：45
|
作者：
Oliveira, Joana [1 ]
da Silva, Mara Alhinho [1 ]
Teixeira, Natercia [1 ]
De Freitas, Victor [1 ]
Salas, Erika [2 ]
机构：
[1] Univ Porto, Dept Quim & Bioquim, REQUIMTE Lab Associado Quim Verde, Fac Ciencias, P-4169007 Oporto, Portugal
[2] Univ Autonoma Chihuahua, Fac Ciencias Quim, Chihuahua 31170, Mexico
来源：
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY | 2015年 / 63卷 / 35期
基金：
芬兰科学院;
关键词：
red grape pomace (GP); malvidin-3-O-coumaroylglucoside; pyranoanthocyanins; anthocyanin oligomers; LC-DAD/MS; MALDI-TOF; VITIS-VINIFERA L; STRUCTURAL-CHARACTERIZATION; ANTIOXIDANT ACTIVITY; BIOACTIVE COMPOUNDS; EXTRACTION; COLOR; CONSTITUENTS; POLYPHENOLS; GRACIANO;
D O I：
10.1021/acs.jafc.5b00256
中图分类号：
S [农业科学];
学科分类号：
09 ;
摘要：
Two phenolic extracts were made from a red wine grape pomace (GP) and fractionated first by sequential liquid liquid extraction with organic solvents. The aqueous fraction was fractionated by low-pressure chromatography on Toyopearl HW-40 gel and on C18. Different fractions were obtained by sequential elution with aqueous/organic solvents, and then analyzed by liquid chromatography and mass spectrometry (LC-DAD/MS and MALDI-TOF). Over SO anthocyanin-based pigments were detected by LC-DAD/MS in GP, mainly pyranoanthocyanins including A- and B-type vitisins and methylpyranoanthocyanins. The presence of oligomeric malvidin-3-O-coumaroylglucoside-based anthocyanins was also detected in GP using both LC-DAD/MS and MALDI-TOF.
引用
收藏
页码：7636 / 7644
页数：9
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