One-pot synthesis of 2-amino-3-cyanopyridine derivatives under solvent-free conditions

被引：20
|
作者：
Ghorbani-Vaghei, Ramin [1 ]
Toghraei-Semiromi, Zahra [1 ]
Karimi-Nami, Rahman [2 ]
机构：
[1] Bu Ali Sina Univ, Dept Organ Chem, Fac Chem, Hamadan 65174, Iran
[2] Univ Tehran, Sch Chem, Univ Coll Sci, Tehran, Iran
来源：
COMPTES RENDUS CHIMIE | 2013年 / 16卷 / 12期
关键词：
2-Amino-3-cyanopyridine; Multicomponent reaction; Aldehyde; Ketone; Malononitrile; Ammonium acetate; Solvent-free; TBBDA; PBBS; MILD; N,N,N',N'-TETRABROMOBENZENE-1,3-DISULFONYLAMIDE; INHIBITORS; DISCOVERY; REAGENTS;
D O I：
10.1016/j.crci.2013.06.006
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A series of 2-amino-3-cyanopyridines were obtained from aryl aldehydes, substituted acetophenones, malononitrile and ammonium acetate in good to excellent yields by proceeding through a simple, mild and efficient procedure utilizing N,N,N ',N '-tetra-bromobenzene-1,3-disulfonamide [TBBDA and poly(N-bromo-N-ethylbenzene-1,3-disulfonamide) IPBBS] as catalysts. (C) 2013 Academie des sciences. Published by Elsevier Masson SAS. All rights reserved.
引用
收藏
页码：1111 / 1117
页数：7
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