Effects of ethanol addition and Ba/Ti ratios on preparation of barium titanate nanocrystals via a spray pyrolysis method

被引：13
|
作者：
Wang, WN
Lenggoro, IW
Okuyama, K [1 ]
Terashi, Y
Wang, YC
机构：
[1] Hiroshima Univ, Grad Sch Engn, Dept Chem Engn, Higashihiroshima 7398527, Japan
[2] Kyocera Corp R&D Ctr, Kagoshima 8994312, Japan
来源：
JOURNAL OF THE AMERICAN CERAMIC SOCIETY | 2006年 / 89卷 / 03期
关键词：
D O I：
10.1111/j.1551-2916.2005.00892.x
中图分类号：
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号：
0805 ; 080502 ;
摘要：
BaTiO3 nanocrystals were synthesized by using a low-pressure spray pyrolysis (SP) method. A new strategy was proposed to improve nanocrystal formation and phase evolution by ethanol addition and Ba/Ti molar ratio variation, respectively. A mixture of submicron and nanoparticles was found with SP of precursors without ethanol addition, while only nanoparticles could be obtained by ethanol addition. BaTiO3 crystal growth was improved by increasing the Ba/Ti ratio. In comparison, SP of the same precursor under atmospheric conditions resulted in only submicron particles with smooth surfaces and irregular morphology.
引用
收藏
页码：888 / 893
页数：6
相关论文
共 41 条
  • [1] Preparation of Ultrafine Barium Titanate Powder by Slurry Spray Pyrolysis
    Lee, Jong Ho
    Hur, Kang Heon
    Lee, Jung Soo
    [J]. JOURNAL OF THE KOREAN CERAMIC SOCIETY, 2009, 46 (02) : 137 - 145
  • [2] Direct Synthesis of Barium Titanate Nanoparticles Via a Low Pressure Spray Pyrolysis Method
    Wei-Ning Wang
    I. Wuled Lenggoro
    Yoshitake Terashi
    Yu-Cong Wang
    Kikuo Okuyama
    [J]. Journal of Materials Research, 2005, 20 : 2873 - 2882
  • [3] Direct synthesis of barium titanate nanoparticles via a low pressure spray pyrolysis method
    Wang, WN
    Lenggoro, IW
    Terashi, Y
    Wang, YC
    Okuyama, K
    [J]. JOURNAL OF MATERIALS RESEARCH, 2005, 20 (10) : 2873 - 2882
  • [4] Nd-doped barium titanate ceramics with various Ti/Ba ratios prepared by sol-gel method
    Shi, QZ
    Cui, B
    Wang, H
    Tian, J
    Chang, ZG
    Hou, YD
    [J]. SCIENCE IN CHINA SERIES B-CHEMISTRY, 2005, 48 (Suppl 1): : 60 - 64
  • [5] Nd-doped barium titanate ceramics with various Ti/Ba ratios prepared by sol-gel method
    SHI Qizhen
    Key Laboratory of Advanced Functional Materials of China Education Ministry
    [J]. Science China Chemistry, 2005, (S1) : 60 - 64
  • [6] Nd-doped barium titanate ceramics with various Ti/Ba ratios prepared by sol-gel method
    Qizhen Shi
    Bin Cui
    Hui Wang
    Jing Tian
    Zhuguo Chang
    Yudong Hou
    [J]. Science in China Series B: Chemistry, 2005, 48 : 60 - 64
  • [7] Nd-doped barium titanate ceramics with various Ti/Ba ratios prepared by sol-gel method
    SHI QizhenCUI BinWANG HuiTIAN JingCHANG Zhuguo HOU Yudong Department of ChemistryNorthwest UniversityShaanxi Key Laboratory of Physicolnorganic ChemistryXian China
    Key Laboratory of Advanced Functional Materials of China Education MinistryBeijing University of TechnologyBeijing China
    [J]. Science in China(Series B:Chemistry)., 2005, (Series B:Chemistry) - 64
  • [8] Preparation of Barium Strontium Titanate Ceramics via Combustion Method
    Bongkarn, T.
    Wicheanrat, C.
    [J]. SMART MATERIALS, 2008, 55-57 : 185 - 188
  • [9] Preparation of spherical, solid barium titanate particles with uniform composition at high precursor concentration by spray pyrolysis
    Gao, L
    Xu, HR
    [J]. JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 2004, 87 (05) : 830 - 833
  • [10] The Preparation of Barium Stannate Titanate Ceramics via Solid State Reaction Method
    Bongkarn, T.
    Khiawwangthong, W.
    [J]. SMART MATERIALS, 2008, 55-57 : 181 - 184
12345