Synthesis, Crystal Structure and Properties of a Silver(I) Complex Constructed from (+)-N-Tosyl-L-glutamic Acid and 1,3-Bis(4-pyridyl)propane
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Zhu Xiao-Yan
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Hebei Normal Univ, Coll Chem & Mat Sci, Shijiazhuang 050024, Peoples R ChinaHebei Normal Univ, Coll Chem & Mat Sci, Shijiazhuang 050024, Peoples R China
Zhu Xiao-Yan
[1
]
Song Hui-Hua
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Hebei Normal Univ, Coll Chem & Mat Sci, Shijiazhuang 050024, Peoples R ChinaHebei Normal Univ, Coll Chem & Mat Sci, Shijiazhuang 050024, Peoples R China
Song Hui-Hua
[1
]
He Rong
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Hebei Normal Univ, Coll Chem & Mat Sci, Shijiazhuang 050024, Peoples R ChinaHebei Normal Univ, Coll Chem & Mat Sci, Shijiazhuang 050024, Peoples R China
He Rong
[1
]
Yu Hai-Tao
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Hebei Normal Univ, Coll Chem & Mat Sci, Shijiazhuang 050024, Peoples R ChinaHebei Normal Univ, Coll Chem & Mat Sci, Shijiazhuang 050024, Peoples R China
Yu Hai-Tao
[1
]
机构:
[1] Hebei Normal Univ, Coll Chem & Mat Sci, Shijiazhuang 050024, Peoples R China
A homochiral complex [Ag(HtsgluO)(bpp)](n) (1) was synthesized and characterized by the reaction of chiral (+)-N-Tosyl-L-glutamic acid (H(2)tsgluO) and 1,3-bis(4-pyridyl)propane (bpp) with silver salts. Single crystal X-ray diffraction analysis reveals that complex 1 crystallizes in the monoclinic space group P2(1), a=1.220 79(18) nm, b=1.034 49(16) rim, c=2.059 5(3) nm, beta=96.006(2)degrees, V=2.586 7(7) nm(3), Z=4, and final R=0.060 2. The silver atom lies in a distorted tetrahedral environment formed by one HtsgluO(-) oxygen, two bpp nitrogen and one symmetry-related silver(I) ions. It exhibits an infinite two-dimensional (2D) layered structure assembled by the argentophilic Ag-Ag interactions. Furthermore, these 2D layers are extended through extensive hydrogen bonding interactions to form an infinite 3D supramolecular network. In addition, the properties of thermogravimetric analysis and photoluminescent behavior of the complex have also been discussed. CCDC: 795083.
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NE Normal Univ, Dept Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R ChinaNE Normal Univ, Dept Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R China
An, HY
Wang, EB
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NE Normal Univ, Dept Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R ChinaNE Normal Univ, Dept Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R China
Wang, EB
Xiao, DR
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NE Normal Univ, Dept Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R ChinaNE Normal Univ, Dept Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R China
Xiao, DR
Li, YG
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NE Normal Univ, Dept Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R ChinaNE Normal Univ, Dept Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R China
Li, YG
Su, ZM
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NE Normal Univ, Dept Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R ChinaNE Normal Univ, Dept Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R China
Su, ZM
Xu, L
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NE Normal Univ, Dept Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R ChinaNE Normal Univ, Dept Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R China
机构:
NE Normal Univ, Dept Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R ChinaNE Normal Univ, Dept Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R China
An, HY
Wang, EB
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机构:
NE Normal Univ, Dept Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R ChinaNE Normal Univ, Dept Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R China
Wang, EB
Xiao, DR
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NE Normal Univ, Dept Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R ChinaNE Normal Univ, Dept Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R China
Xiao, DR
Li, YG
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机构:
NE Normal Univ, Dept Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R ChinaNE Normal Univ, Dept Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R China
Li, YG
Su, ZM
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机构:
NE Normal Univ, Dept Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R ChinaNE Normal Univ, Dept Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R China
Su, ZM
Xu, L
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机构:
NE Normal Univ, Dept Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R ChinaNE Normal Univ, Dept Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R China