Preparation and characterization of neodymium hydroxide powder via the hydration method

被引：0
|
作者：
Li, Hongxi [1 ]
Xu, Chenggong [1 ]
Yang, Qishan [1 ]
机构：
[1] Inner Mongolia Univ Sci & Technol, Sch Chem & Chem Engn, Baotou 014010, Peoples R China
来源：
CHINESE JOURNAL OF CHEMICAL ENGINEERING | 2020年 / 28卷 / 07期
关键词：
Hydration method; Neodymium hydroxide; Powder preparation; Influencing factor; Green chemical engineering; OXIDE NANORODS; ND(OH)(3); ND; LA(OH)(3); LANTHANUM; PR; EU; GD; SM;
D O I：
10.1016/j.cjche.2020.04.018
中图分类号：
TQ [化学工业];
学科分类号：
0817 ;
摘要：
The preparation of Nd(OH)(3) powder by the direct hydration method using Nd2O3 as a raw material was studied, and the effects of stirring mode, H2O and Nd2O3 molar ratio, stirring rate, and reaction time on temperature change and conversion rate in a hydration system were analyzed. The reasonable process conditions for the direct hydration of Nd(OH)(3) by Nd2O3 were then determined. Process, morphology, and structure were considered in the preparation of neodymium hydroxide powder, and its composition was investigated by X-ray powder diffraction, scanning electron microscopy, laser particle size analysis, therrnogravimetric differential thermal analysis, and chemical analysis. It has been proved that the process is simple and feasible, in line with the concept of modem green chemistry, and the products also meet the market requirements. (C) 2020 The Chemical Industry and Engineering Society of China, and Chemical Industry Press Co., Ltd. All rights reserved.
引用
收藏
页码：1973 / 1980
页数：8
相关论文
共 50 条
  • [1] Preparation and characterization of neodymium hydroxide powder via the hydration method
    Hongxi Li
    Chenggong Xu
    Qishan Yang
    Chinese Journal of Chemical Engineering, 2020, 28 (07) : 1973 - 1980
  • [2] PREPARATION OF NEODYMIUM HYDROXIDE NANORODS AND NEODYMIUM OXIDE NANORODS BY A HYDROTHERMAL METHOD
    Ekthammathat, N.
    Phuruangrat, A.
    Kuntalue, B.
    Thongtem, S.
    Thongtem, T.
    DIGEST JOURNAL OF NANOMATERIALS AND BIOSTRUCTURES, 2015, 10 (02) : 715 - 719
  • [3] Jet cavitation-enhanced hydration method for the preparation of magnesium hydroxide
    Zuo, Maosheng
    Yu, Honglei
    Wang, Dexi
    Fan, Lihua
    CHEMICAL ENGINEERING AND PROCESSING-PROCESS INTENSIFICATION, 2024, 205
  • [4] Preparation and characterization of nano-ZnO powder via Polymer gelation method
    Salehi, Amir
    Rohani, Aliasghar
    Manafi, Sahebali
    Tabrizi, Mahmood
    Fardafshari, Amin
    INTERNATIONAL JOURNAL OF PLASTICS TECHNOLOGY, 2011, 15 (01) : 43 - 51
  • [5] Synthesis and characterization of neodymium hydroxide and oxide nanowires
    Huang, PX
    He, B
    Wu, F
    Pan, GL
    Gao, XP
    CHINESE JOURNAL OF INORGANIC CHEMISTRY, 2006, 22 (04) : 639 - 644
  • [6] PREPARATION OF NEODYMIUM HYDROXIDE BY VAPOR-PHASE REACTION
    KUWANO, Y
    SHIROKI, KI
    JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1972, 55 (07) : 378 - &
  • [7] Preparation and characterization of polystyrene/neodymium hydroxide (PS/Nd(OH)3) nano-composites
    Alsewailem, Fares D.
    Bagabas, Abdulaziz A.
    Binkhodor, Yazeed A.
    MATERIALS RESEARCH EXPRESS, 2018, 5 (03)
  • [8] Preparation and characterization of surface modified powder of calcium hydroxide used as chlorine scavenger
    Chang, Honghong
    Cui, Longhui
    Li, Xing
    Shen, Jun
    Wei, Wenlong
    Kou, Ziming
    JOURNAL OF LOSS PREVENTION IN THE PROCESS INDUSTRIES, 2012, 25 (06) : 1028 - 1032
  • [9] The effect of powder preparation method on the artificial photosynthesis activities of neodymium doped titania powders
    Yurtsever, Husnu Arda
    Ciftcioglu, Muhsin
    INTERNATIONAL JOURNAL OF HYDROGEN ENERGY, 2018, 43 (44) : 20162 - 20175
  • [10] Preparation of lamellar magnesium hydroxide nanoparticles via precipitation method
    Jiang, Wenjun
    Hua, Xiao
    Han, Qiaofeng
    Yang, Xujie
    Lu, Lude
    Wang, Xin
    POWDER TECHNOLOGY, 2009, 191 (03) : 227 - 230
12345