A low temperature co-precipitation preparation of nano-sized zinc containing β-tricalcium phosphate powders

被引：1
|
作者：
Miao, SD [1 ]
Weng, WJ [1 ]
Cheng, K [1 ]
Song, CL [1 ]
Du, PY [1 ]
Zhao, GL [1 ]
Shen, G [1 ]
Wang, JX [1 ]
Han, GR [1 ]
机构：
[1] Zhejiang Univ, Dept Mat Sci & Engn, Hangzhou 310027, Peoples R China
来源：
BIOCERAMICS 18, PTS 1 AND 2 | 2006年 / 309-311卷
关键词：
zinc containing; beta-tricalcium phosphate; nano-sized powder; preparation;
D O I：
10.4028/www.scientific.net/KEM.309-311.565
中图分类号：
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号：
0805 ; 080502 ;
摘要：
Nano-sized zinc containing beta-tricalcium phosphate (ZnTCP) powders were synthesized by a co-precipitation method. The co-precipitation took place in an ice-water bathed beaker, after further washing, freezing, lyophilizing and calcining at 800 degrees C, the precipitates transformed to ZnTCP powders. The XRD pattern of the ZnTCP powders demonstrated a pure beta-TCP phase. TEM observation revealed the particle size is about 100-120nm, which is favorable for TCP particles to form composites, such as polymer based composite, and as well to attain a desired microstructure. It was found zinc incorporation could eventually result in the decrease of particle size, thus be beneficial for its further application.
引用
收藏
页码：565 / 568
页数：4
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